13-(3-chlorophenyl)-3,3-dimethyl-2,3,4,13-tetrahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

Base Information

Chemical Name:13-(3-chlorophenyl)-3,3-dimethyl-2,3,4,13-tetrahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione
CAS No.:1173891-46-7
Molecular Formula:C₂₃H₁₉ClN₂O₃
Molecular Weight:406.868
Hs Code.:

Synonyms:13-(3-chlorophenyl)-3,3-dimethyl-2,3,4,13-tetrahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

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Chemical Property of 13-(3-chlorophenyl)-3,3-dimethyl-2,3,4,13-tetrahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

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Technology Process of 13-(3-chlorophenyl)-3,3-dimethyl-2,3,4,13-tetrahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

There total 4 articles about 13-(3-chlorophenyl)-3,3-dimethyl-2,3,4,13-tetrahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 85-44-9
phthalic anhydride

: 126-81-8
dimedone

: 587-04-2
m-Chlorobenzaldehyde

: 1173891-46-7
13-(3-chlorophenyl)-3,3-dimethyl-2,3,4,13-tetrahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

Guidance literature:: With hydrazine hydrate; In neat (no solvent); at 80 ℃; for 0.2h; Green chemistry;
DOI:10.1002/jhet.3989

Reference yield: 94.0%

: 1445-69-8
2,3-dihydrophthalazine-1,4-dione

: 126-81-8
dimedone

: 587-04-2
m-Chlorobenzaldehyde

: 1173891-46-7
13-(3-chlorophenyl)-3,3-dimethyl-2,3,4,13-tetrahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

Guidance literature:: With silica-supported tungstic acid; In neat (no solvent); at 80 ℃; for 0.566667h; Green chemistry;
DOI:10.1080/10426507.2019.1661414

Reference yield: 91.0%

: 85-44-9
phthalic anhydride

: 126-81-8
dimedone

: 7803-57-8,79785-97-0
hydrazine hydrate

: 587-04-2
m-Chlorobenzaldehyde

: 1173891-46-7
13-(3-chlorophenyl)-3,3-dimethyl-2,3,4,13-tetrahydro-1H-indazolo[1,2-b]phthalazine-1,6,11-trione

Guidance literature:: With cobalt ferrite chitosan sulfonic acid magnetic nanoparticle; In neat (no solvent); at 80 ℃; for 7h; Green chemistry;
DOI:10.1039/c4ra09984b