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Technology Process of [H(C20H8N4Zn(C6H3(OC2H4C(CH3)3)2)2CC)2H]

[H(C20H8N4Zn(C6H3(OC2H4C(CH3)3)2)2CC)2H]

Base Information
  • Chemical Name:[H(C20H8N4Zn(C6H3(OC2H4C(CH3)3)2)2CC)2H]
  • CAS No.:944244-96-6
  • Molecular Formula:C116H134N8O8Zn2
  • Molecular Weight:1899.17
  • Hs Code.:
[H(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Zn(C<sub>6</sub>H<sub>3</sub>(OC<sub>2</sub>H<sub>4</sub>C(CH<sub>3</sub>)3)2)2CC)2H]

Synonyms:[H(C20H8N4Zn(C6H3(OC2H4C(CH3)3)2)2CC)2H]

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Chemical Property of [H(C20H8N4Zn(C6H3(OC2H4C(CH3)3)2)2CC)2H]
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Technology Process of [H(C20H8N4Zn(C6H3(OC2H4C(CH3)3)2)2CC)2H]

There total 1 articles about [H(C20H8N4Zn(C6H3(OC2H4C(CH3)3)2)2CC)2H] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C<sub>125</sub>H<sub>154</sub>N<sub>8</sub>O<sub>8</sub>SiZn<sub>2</sub>

C125H154N8O8SiZn2

[H(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Zn(C<sub>6</sub>H<sub>3</sub>(OC<sub>2</sub>H<sub>4</sub>C(CH<sub>3</sub>)3)2)2CC)2H]
944244-96-6

[H(C20H8N4Zn(C6H3(OC2H4C(CH3)3)2)2CC)2H]

Guidance literature:
With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 0.25h;
DOI:10.1039/d0sc03446k

Reference yield:

4,7-dibromobenzo[c][1,2,5]thiadiazole
15155-41-6

4,7-dibromobenzo[c][1,2,5]thiadiazole

[H(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Zn(C<sub>6</sub>H<sub>3</sub>(OC<sub>2</sub>H<sub>4</sub>C(CH<sub>3</sub>)3)2)2CC)2H]
944244-96-6

[H(C20H8N4Zn(C6H3(OC2H4C(CH3)3)2)2CC)2H]

C<sub>122</sub>H<sub>135</sub>BrN<sub>10</sub>O<sub>8</sub>SZn<sub>2</sub>

C122H135BrN10O8SZn2

Guidance literature:
With tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; In tetrahydrofuran; at 60 ℃; for 12h;
DOI:10.1039/d0sc03446k

Reference yield:

ammonium hexafluorophosphate

ammonium hexafluorophosphate

[Ru(2,2':6',2''-terpyridine)(4'-bromo-2,2':6',2''-terpyridine)]<sup>(2+)</sup>
211450-15-6

[Ru(2,2':6',2''-terpyridine)(4'-bromo-2,2':6',2''-terpyridine)](2+)

[H(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Zn(C<sub>6</sub>H<sub>3</sub>(OC<sub>2</sub>H<sub>4</sub>C(CH<sub>3</sub>)3)2)2CC)2H]
944244-96-6

[H(C20H8N4Zn(C6H3(OC2H4C(CH3)3)2)2CC)2H]

[(H(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Zn(C<sub>6</sub>H<sub>3</sub>(OC<sub>2</sub>H<sub>4</sub>C(CH<sub>3</sub>)3)2)2C<sub>2</sub>)2C<sub>5</sub>H<sub>2</sub>N(C<sub>5</sub>H<sub>4</sub>N)2)Ru(C<sub>5</sub>H<sub>3</sub>N(C<sub>5</sub>H<sub>4</sub>N)2)]<sup>(2+)</sup>*2PF<sub>6</sub><sup>(1-)</sup>=C<sub>146</sub>H<sub>154</sub>F<sub>12</sub>N<sub>14</sub>O<sub>8</sub>P<sub>2</sub>RuZn<sub>2</sub>

[(H(C20H8N4Zn(C6H3(OC2H4C(CH3)3)2)2C2)2C5H2N(C5H4N)2)Ru(C5H3N(C5H4N)2)](2+)*2PF6(1-)=C146H154F12N14O8P2RuZn2

Guidance literature:
With Pd2(dibenzylideneacetone)3; As(C6H5)3; In further solvent(s); Ru and Zn complexes reacted in the presence of Pd2(dba)3 and AsPh3 in MeCN/THF/TEA at 60°C for 7 h; chromd. (silica, MeCN/H2O/aq. KNO3), treated with NH4PF6;
DOI:10.1021/ja0707512
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