2-[bis(2-bromoethyl)amino]-N-ethyl-N-(2-hydroxyethyl)-3,5-dinitrobenzamide

Base Information

Chemical Name:2-[bis(2-bromoethyl)amino]-N-ethyl-N-(2-hydroxyethyl)-3,5-dinitrobenzamide
CAS No.:1221752-03-9
Molecular Formula:C₁₅H₂₀Br₂N₄O₆
Molecular Weight:512.155
Hs Code.:

Synonyms:2-[bis(2-bromoethyl)amino]-N-ethyl-N-(2-hydroxyethyl)-3,5-dinitrobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[bis(2-bromoethyl)amino]-N-ethyl-N-(2-hydroxyethyl)-3,5-dinitrobenzamide

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Technology Process of 2-[bis(2-bromoethyl)amino]-N-ethyl-N-(2-hydroxyethyl)-3,5-dinitrobenzamide

There total 1 articles about 2-[bis(2-bromoethyl)amino]-N-ethyl-N-(2-hydroxyethyl)-3,5-dinitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1221752-45-9
2-[bis(2-chloroethyl)amino]-N-ethyl-N-(2-hydroxyethyl)-3,5-dinitrobenzamide

: 1221752-03-9
2-[bis(2-bromoethyl)amino]-N-ethyl-N-(2-hydroxyethyl)-3,5-dinitrobenzamide

Guidance literature:: With lithium bromide; In butanone; for 3h; Heating; Reflux;

Reference yield: 88.0%

: 1221752-03-9
2-[bis(2-bromoethyl)amino]-N-ethyl-N-(2-hydroxyethyl)-3,5-dinitrobenzamide

: 137348-86-8
di-tert-butyl diisopropylphosphoramide

: 1221752-58-4
2-[{2-[bis(2-bromoethyl)amino]-3,5-dinitrobenzoyl}(ethyl)amino]ethyl di(tert-butyl) phosphate

Guidance literature:: 2-[bis(2-bromoethyl)amino]-N-ethyl-N-(2-hydroxyethyl)-3,5-dinitrobenzamide; di-tert-butyl diisopropylphosphoramide; With 1H-tetrazole; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃; for 3h; Inert atmosphere;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile; at -15 - 20 ℃; for 2h;