(E)-[1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-yl]-methylamine

Base Information

• Chemical Name: (E)-[1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-yl]-methylamine
• CAS No.: 1020106-74-4
• Molecular Formula: C₂₀H₂₁Cl₂N₃S
• Molecular Weight: 406.379

Synonyms:(E)-[1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-yl]-methylamine

Chemical Property of (E)-[1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-yl]-methylamine

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Technology Process of (E)-[1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-yl]-methylamine

There total 2 articles about (E)-[1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-yl]-methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

→ (E)-[1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-yl]-methylamine (1020106-74-4)

Guidance literature:

Reference yield: 71.0%

3-azidomethyl-1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazole (1020106-73-3) → (E)-[1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-yl]-methylamine (1020106-74-4)

Guidance literature:

With water; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 48h; Staudinger reduction;

DOI:10.1039/b716434c

Reference yield: 78.0%

3,3-dimethylbutanoic acid chloride (7065-46-5) + (E)-[1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-yl]-methylamine (1020106-74-4) → N-[1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-ylmethyl]-3,3-dimethyl-butyramide

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1039/b716434c

upstream raw materials:

3-azidomethyl-1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazole

Downstream raw materials:

pyridine-2-carboxylic acid [1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-ylmethyl]-amide

1-[1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-ylmethyl]-3-propyl-urea

N-[1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-ylmethyl]-2-thiophen-2-yl-acetamide

cyclopentanecarboxylic acid [1-(2,4-dichloro-phenyl)-4-methyl-5-(5-pent-1-enyl-thiophen-2-yl)-1H-pyrazol-3-ylmethyl]-amide

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