C₉H₁₄O₄C₈H₈O

Base Information

Chemical Name:C₉H₁₄O₄C₈H₈O
CAS No.:956964-09-3
Molecular Formula:C₁₇H₂₂O₅
Molecular Weight:306.359
Hs Code.:

C<sub>9</sub>H<sub>14</sub>O<sub>4</sub>C<sub>8</sub>H<sub>8</sub>O

Synonyms:C₉H₁₄O₄C₈H₈O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₉H₁₄O₄C₈H₈O

Chemical Property:

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Technology Process of C₉H₁₄O₄C₈H₈O

There total 9 articles about C₉H₁₄O₄C₈H₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [(3aS,4E,5S,6aR)-4-ethylidene-2,2-dimethyltetrahydro-3aH-cyclopenta[d][1,3]dioxol-5-yl]acetic acid 3-hydroxyphenethyl ester

: 956964-09-3
C₉H₁₄O₄C₈H₈O

Guidance literature:: With hydrogenchloride; In water; acetonitrile; at 23 ℃;
DOI:10.1021/jo071146k

Reference yield:

: 115509-13-2
(3aR,6aR)-2,2-Dimethyl-3a,6a-dihydro-cyclopenta[1,3]dioxol-4-one

: 956964-09-3
C₉H₁₄O₄C₈H₈O

Guidance literature:: Multi-step reaction with 7 steps

1: 95 percent / hydrogen / Pd/C / ethyl acetate / 20 °C

2: 57 percent / LHMDS; HMPA; Me₂Zn / tetrahydrofuran; toluene / -78 - -45 °C

3: KHMDS; CeCl₃ / tetrahydrofuran / -45 °C

4: 100 percent / LiOH / tetrahydrofuran; methanol; H₂O / 1 h / 20 °C

5: 82 percent / N,N'-dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂ / 0 - 23 °C

6: tetrabutylammonium fluoride; hydrofluoric acid / tetrahydrofuran; H₂O / 0 °C / pH 6.5 - 7.0

7: aq. HCl / acetonitrile; H₂O / 23 °C

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; lithium hydroxide; cerium(III) chloride; hydrogen fluoride; tetrabutyl ammonium fluoride; hydrogen; dimethyl zinc(II); potassium hexamethylsilazane; dicyclohexyl-carbodiimide; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; toluene; acetonitrile; 3: Wittig reaction;
DOI:10.1021/jo071146k

Reference yield:

: 683276-43-9
(4R,5R)-1-(2,2-dimethyl-5-vinyl-[1,3]dioxolan-4-yl)prop-2-en-1-ol

: 956964-09-3
C₉H₁₄O₄C₈H₈O

Guidance literature:: Multi-step reaction with 8 steps

1.1: Grubbs catalyst / CH₂Cl₂ / 4 h / 23 °C

1.2: 87 percent / pyridinium chlorochromate / CH₂Cl₂ / 12 h / 23 °C

2.1: 95 percent / hydrogen / Pd/C / ethyl acetate / 20 °C

3.1: 57 percent / LHMDS; HMPA; Me₂Zn / tetrahydrofuran; toluene / -78 - -45 °C

4.1: KHMDS; CeCl₃ / tetrahydrofuran / -45 °C

5.1: 100 percent / LiOH / tetrahydrofuran; methanol; H₂O / 1 h / 20 °C

6.1: 82 percent / N,N'-dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂ / 0 - 23 °C

7.1: tetrabutylammonium fluoride; hydrofluoric acid / tetrahydrofuran; H₂O / 0 °C / pH 6.5 - 7.0

8.1: aq. HCl / acetonitrile; H₂O / 23 °C

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; lithium hydroxide; cerium(III) chloride; hydrogen fluoride; tetrabutyl ammonium fluoride; hydrogen; dimethyl zinc(II); potassium hexamethylsilazane; dicyclohexyl-carbodiimide; lithium hexamethyldisilazane; palladium on activated charcoal; Grubbs catalyst first generation; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; toluene; acetonitrile; 4.1: Wittig reaction;
DOI:10.1021/jo071146k