[C₆H₅CH₂P(C₆H₅)3]⁽¹⁺⁾*[(CN)(Au(C₆F₅))2]^(1-)=[C₆H₅CH₂P(C₆H₅)3][(CN)(Au(C₆F₅))2]

Base Information

• Chemical Name: [C₆H₅CH₂P(C₆H₅)3]⁽¹⁺⁾*[(CN)(Au(C₆F₅))2]^(1-)=[C₆H₅CH₂P(C₆H₅)3][(CN)(Au(C₆F₅))2]
• CAS No.: 80330-61-6
• Molecular Formula: C₁₃Au₂F₁₀N*C₂₅H₂₂P
• Molecular Weight: 1107.49

Synonyms:[C₆H₅CH₂P(C₆H₅)3]⁽¹⁺⁾*[(CN)(Au(C₆F₅))2]^(1-)=[C₆H₅CH₂P(C₆H₅)3][(CN)(Au(C₆F₅))2]

Chemical Property of [C₆H₅CH₂P(C₆H₅)3]⁽¹⁺⁾*[(CN)(Au(C₆F₅))2]^(1-)=[C₆H₅CH₂P(C₆H₅)3][(CN)(Au(C₆F₅))2]

Chemical Property:

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Technology Process of [C₆H₅CH₂P(C₆H₅)3]⁽¹⁺⁾*[(CN)(Au(C₆F₅))2]^(1-)=[C₆H₅CH₂P(C₆H₅)3][(CN)(Au(C₆F₅))2]

There total 3 articles about [C₆H₅CH₂P(C₆H₅)3]⁽¹⁺⁾*[(CN)(Au(C₆F₅))2]^(1-)=[C₆H₅CH₂P(C₆H₅)3][(CN)(Au(C₆F₅))2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

[C6H5CH2P(C6H5)3](1+)*[Au(C6F5)(CN)](1-)=[C6H5CH2P(C6H5)3Au(C6F5)(CN)] (80319-90-0) → [C6H5CH2P(C6H5)3](1+)*[(CN)(Au(C6F5))2](1-)=[C6H5CH2P(C6H5)3][(CN)(Au(C6F5))2] (80330-61-6)

Guidance literature:

With AgClO₄; In dichloromethane; stirring for 1 h; ppt. was removed, evapn. of filtrate to dryness, treated with ether, ppt. filtered, evapn. of filtrate to dryness, recrystn. from CH2Cl2/hexane, elem. anal.;

DOI:10.1016/S0022-328X(00)86109-4

Reference yield:

pentafluorophenyl(tetrahydrothiophene)gold(I) → [C6H5CH2P(C6H5)3](1+)*[(CN)(Au(C6F5))2](1-)=[C6H5CH2P(C6H5)3][(CN)(Au(C6F5))2] (80330-61-6)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium cyanide / methanol

2: AgClO₄ / dichloromethane

With potassium cyanide; AgClO₄; In methanol; dichloromethane;

DOI:10.1016/S0022-328X(00)86109-4

Reference yield:

triphenyl benzyl phosphonium perchlorate (19879-94-8) → [C6H5CH2P(C6H5)3](1+)*[(CN)(Au(C6F5))2](1-)=[C6H5CH2P(C6H5)3][(CN)(Au(C6F5))2] (80330-61-6)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium cyanide / methanol

2: AgClO₄ / dichloromethane

With potassium cyanide; AgClO₄; In methanol; dichloromethane;

DOI:10.1016/S0022-328X(00)86109-4

upstream raw materials:

[C₆H₅CH₂P(C₆H₅)3]⁽¹⁺⁾*[Au(C₆F₅)(CN)]^(1-)=[C₆H₅CH₂P(C₆H₅)3Au(C₆F₅)(CN)]

triphenyl benzyl phosphonium perchlorate

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