1,3-Benzodithiol-2-ylidenetriphenylphosphorane

Base Information

Chemical Name:1,3-Benzodithiol-2-ylidenetriphenylphosphorane
CAS No.:62217-36-1
Molecular Formula:C₂₅H₁₉PS₂
Molecular Weight:414.532
Hs Code.:
DSSTox Substance ID:DTXSID401245544
Nikkaji Number:J2.721.861J

Synonyms:DTXSID401245544;62217-36-1;1,3-Benzodithiol-2-ylidenetriphenylphosphorane

Suppliers and Price of 1,3-Benzodithiol-2-ylidenetriphenylphosphorane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,3-Benzodithiol-2-ylidenetriphenylphosphorane

Chemical Property:

XLogP3:6.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:414.06657995
Heavy Atom Count:28
Complexity:499

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(=C2SC3=CC=CC=C3S2)(C4=CC=CC=C4)C5=CC=CC=C5

Technology Process of 1,3-Benzodithiol-2-ylidenetriphenylphosphorane

There total 2 articles about 1,3-Benzodithiol-2-ylidenetriphenylphosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117156-71-5
C₂₅H₂₀PS₂⁽¹⁺⁾*F₆P^(1-)

: 62217-36-1
(1,3-benzodithiol-2-ylidene)triphenylphosphorane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -80 ℃; for 2h;

Reference yield:

: 62217-36-1
(1,3-benzodithiol-2-ylidene)triphenylphosphorane

Guidance literature:: Salz 2a, n-BuLi;

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 62217-36-1
(1,3-benzodithiol-2-ylidene)triphenylphosphorane

: 934-36-1
2-thioxo-1,3-benzodithiole

: 24648-13-3
dibenzotetrathiafulvalene

: 80541-37-3
3-Benzo[1,3]dithiol-2-ylidene-benzo[1,4]dithiine-2-thione

: 3878-45-3
triphenylphosphine sulfide

Guidance literature:: With p-toluidine; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg, 2 h, 2.) THF, -78 deg, 2 h;
DOI:10.1246/bcsj.54.2845