1-[3-(4-methoxybenzyloxy)propyl]-1-methyl-2-methylidene-1-silacyclohexane

Base Information

Chemical Name:1-[3-(4-methoxybenzyloxy)propyl]-1-methyl-2-methylidene-1-silacyclohexane
CAS No.:1053230-40-2
Molecular Formula:C₁₈H₂₈O₂Si
Molecular Weight:304.505
Hs Code.:

Synonyms:1-[3-(4-methoxybenzyloxy)propyl]-1-methyl-2-methylidene-1-silacyclohexane

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Chemical Property of 1-[3-(4-methoxybenzyloxy)propyl]-1-methyl-2-methylidene-1-silacyclohexane

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Technology Process of 1-[3-(4-methoxybenzyloxy)propyl]-1-methyl-2-methylidene-1-silacyclohexane

There total 2 articles about 1-[3-(4-methoxybenzyloxy)propyl]-1-methyl-2-methylidene-1-silacyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 919801-00-6
1-chloro-1-methyl-2-methylidene-1-silacyclohexane

: 147193-45-1
1-[(3-bromopropoxy)methyl]-4-methoxybenzene

: 1053230-40-2
1-[3-(4-methoxybenzyloxy)propyl]-1-methyl-2-methylidene-1-silacyclohexane

Guidance literature:: 1-[(3-bromopropoxy)methyl]-4-methoxybenzene; With magnesium; In tetrahydrofuran; at 60 ℃; Inert atmosphere;

1-chloro-1-methyl-2-methylidene-1-silacyclohexane; In tetrahydrofuran; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1002/ejoc.200800305

Reference yield: 15.0%

: 87280-36-2
2,6-dibromohex-1-ene

: 1053230-42-4
diethoxy[3-(4-methoxybenzyloxy)propyl]methylsilane

: 1053230-40-2
1-[3-(4-methoxybenzyloxy)propyl]-1-methyl-2-methylidene-1-silacyclohexane

Guidance literature:: 2,6-dibromohex-1-ene; With lithium; In diethyl ether; at -5 ℃; for 14h; Inert atmosphere;

diethoxy[3-(4-methoxybenzyloxy)propyl]methylsilane; In diethyl ether; at 20 ℃; for 10h; Inert atmosphere;
DOI:10.1002/ejoc.200800305