(2S)-2-(4-(N-Boc-N-2-picolylaminomethyl) benzoyl)-5-(imidazol-2-yl)aminovalerate (1'S)-1'-(1-naphthyl) ethylamide

Base Information

Chemical Name:(2S)-2-(4-(N-Boc-N-2-picolylaminomethyl) benzoyl)-5-(imidazol-2-yl)aminovalerate (1'S)-1'-(1-naphthyl) ethylamide
CAS No.:369656-63-3
Molecular Formula:C₃₉H₄₅N₇O₄
Molecular Weight:675.831
Hs Code.:

Synonyms:(2S)-2-(4-(N-Boc-N-2-picolylaminomethyl) benzoyl)-5-(imidazol-2-yl)aminovalerate (1'S)-1'-(1-naphthyl) ethylamide

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Chemical Property of (2S)-2-(4-(N-Boc-N-2-picolylaminomethyl) benzoyl)-5-(imidazol-2-yl)aminovalerate (1'S)-1'-(1-naphthyl) ethylamide

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Technology Process of (2S)-2-(4-(N-Boc-N-2-picolylaminomethyl) benzoyl)-5-(imidazol-2-yl)aminovalerate (1'S)-1'-(1-naphthyl) ethylamide

There total 1 articles about (2S)-2-(4-(N-Boc-N-2-picolylaminomethyl) benzoyl)-5-(imidazol-2-yl)aminovalerate (1'S)-1'-(1-naphthyl) ethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-aminoimidazole hemisulfate

: 369656-62-2
N-[(1S)-1-(1-naphthyl)ethyl]-5-hydroxy-2-(S)-[4-[N-Boc-N-(pyridin-2-ylmethyl)aminomethyl]benzoylamino]pentanoylamide

: 369656-63-3
(2S)-2-(4-(N-Boc-N-2-picolylaminomethyl) benzoyl)-5-(imidazol-2-yl)aminovalerate (1'S)-1'-(1-naphthyl) ethylamide

Guidance literature:: N-[(1S)-1-(1-naphthyl)ethyl]-5-hydroxy-2-(S)-[4-[N-Boc-N-(pyridin-2-ylmethyl)aminomethyl]benzoylamino]pentanoylamide; With N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate; In chloroform; water; at 20 ℃; for 5h;

2-aminoimidazole hemisulfate; With triethylamine; In methanol; pH=8; Molecular sieve;

With sodium cyanoborohydride; acetic acid; In methanol; for 96h; pH=6 - 7;

Reference yield:

: 369656-63-3
(2S)-2-(4-(N-Boc-N-2-picolylaminomethyl) benzoyl)-5-(imidazol-2-yl)aminovalerate (1'S)-1'-(1-naphthyl) ethylamide

: (2S)-2-(4-(2-picolylamino methyl) benzoyl)-5-(imidazol-2-yl) aminovalerate (1'S)-1'-(1-naphthyl) ethylamide hydrochloride

Guidance literature:: (2S)-2-(4-(N-Boc-N-2-picolylaminomethyl) benzoyl)-5-(imidazol-2-yl)aminovalerate (1'S)-1'-(1-naphthyl) ethylamide; With hydrogenchloride; In 1,4-dioxane; methanol; at 20 ℃; for 2h;

With hydrogenchloride; In water;