(2R,3R,4S,5R,6R)-3,4-Bis-benzyloxy-6-benzyloxymethyl-5-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran

Base Information

Chemical Name:(2R,3R,4S,5R,6R)-3,4-Bis-benzyloxy-6-benzyloxymethyl-5-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran
CAS No.:215439-76-2
Molecular Formula:C₄₁H₆₂O₇Si₂
Molecular Weight:723.11
Hs Code.:

(2R,3R,4S,5R,6R)-3,4-Bis-benzyloxy-6-benzyloxymethyl-5-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran

Synonyms:(2R,3R,4S,5R,6R)-3,4-Bis-benzyloxy-6-benzyloxymethyl-5-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran

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Chemical Property of (2R,3R,4S,5R,6R)-3,4-Bis-benzyloxy-6-benzyloxymethyl-5-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran

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Technology Process of (2R,3R,4S,5R,6R)-3,4-Bis-benzyloxy-6-benzyloxymethyl-5-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran

There total 1 articles about (2R,3R,4S,5R,6R)-3,4-Bis-benzyloxy-6-benzyloxymethyl-5-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 89031-84-5
3-(tert-butyldimethylsilyloxy)propyl bromide

: 117253-05-1
2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 215439-76-2
(2R,3R,4S,5R,6R)-3,4-Bis-benzyloxy-6-benzyloxymethyl-5-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran

Guidance literature:: With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 3h;
DOI:10.1039/a804272a

Reference yield: 97.0%

: 215439-76-2
(2R,3R,4S,5R,6R)-3,4-Bis-benzyloxy-6-benzyloxymethyl-5-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran

: 215439-78-4
3-[(2R,3R,4S,5R,6R)-4,5-Bis-benzyloxy-2-benzyloxymethyl-6-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yloxy]-propan-1-ol

Guidance literature:: With water; toluene-4-sulfonic acid; In acetonitrile; for 1.5h; Ambient temperature;
DOI:10.1039/a804272a

Reference yield:

: 215439-76-2
(2R,3R,4S,5R,6R)-3,4-Bis-benzyloxy-6-benzyloxymethyl-5-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran

: 215439-85-3
2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzyl-4-O-{3-[6-O-(tert-butyldiphenylsilyl)-2-deoxy-3,4-di-O-(p-methylbenzoyl)-2-phthalimido-β-D-glucopyranosyloxy]propyl}-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / H₂O, p-TsOH / acetonitrile / 1.5 h / Ambient temperature

2: 85 percent / NIS, AgOTf, molecular sieves 4 Angstroem / toluene / 1 h / 0 °C

With N-iodo-succinimide; 4 A molecular sieve; water; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; In toluene; acetonitrile;
DOI:10.1039/a804272a