C₁₄H₂₂N₄O₃

Base Information

Chemical Name:C₁₄H₂₂N₄O₃
CAS No.:1569084-03-2
Molecular Formula:C₁₄H₂₂N₄O₃
Molecular Weight:294.354
Hs Code.:

C<sub>14</sub>H<sub>22</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:C₁₄H₂₂N₄O₃

Suppliers and Price of C₁₄H₂₂N₄O₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₄H₂₂N₄O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₄H₂₂N₄O₃

There total 6 articles about C₁₄H₂₂N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1569084-02-1
C₁₆H₂₄N₂O₄

: 1569084-03-2
C₁₄H₂₂N₄O₃

Guidance literature:: With hydrazine hydrate; In ethanol; at 100 ℃; for 4h;

Reference yield:

: 73368-41-9
4-amino-3-methoxybenzoic acid ethyl ester

: 1569084-03-2
C₁₄H₂₂N₄O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetonitrile / 24 h / 100 °C / Autoclave

2.1: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 40 °C

3.1: HATU; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 20 °C

3.2: 15 h / 20 °C

4.1: hydrazine hydrate / ethanol / 4 h / 100 °C

With hydrazine hydrate; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; HATU; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile;

Reference yield:

: 5081-36-7
3-methoxy-4-nitrobenzoic acid

: 1569084-03-2
C₁₄H₂₂N₄O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / 14 h / 60 °C

2.1: palladium on activated charcoal; hydrogen / ethanol / 12 h / 20 °C

3.1: potassium carbonate / acetonitrile / 24 h / 100 °C / Autoclave

4.1: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 40 °C

5.1: HATU; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 20 °C

5.2: 15 h / 20 °C

6.1: hydrazine hydrate / ethanol / 4 h / 100 °C

With thionyl chloride; hydrazine hydrate; palladium on activated charcoal; water; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; HATU; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile;