1,12-Bis(2,6,6-trimethylcyclohex-1-enyl)-3,6,10-trimethyldodeca-1,3,5,7,9,11-hexaene

Base Information

Chemical Name:1,12-Bis(2,6,6-trimethylcyclohex-1-enyl)-3,6,10-trimethyldodeca-1,3,5,7,9,11-hexaene
CAS No.:82848-18-8
Molecular Formula:C₃₃H₄₈
Molecular Weight:444.744
Hs Code.:

Synonyms:1,12-Bis(2,6,6-trimethylcyclohex-1-enyl)-3,6,10-trimethyldodeca-1,3,5,7,9,11-hexaene

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Chemical Property of 1,12-Bis(2,6,6-trimethylcyclohex-1-enyl)-3,6,10-trimethyldodeca-1,3,5,7,9,11-hexaene

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Technology Process of 1,12-Bis(2,6,6-trimethylcyclohex-1-enyl)-3,6,10-trimethyldodeca-1,3,5,7,9,11-hexaene

There total 5 articles about 1,12-Bis(2,6,6-trimethylcyclohex-1-enyl)-3,6,10-trimethyldodeca-1,3,5,7,9,11-hexaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 116-31-4
all-trans-Retinal

: 77837-61-7
(β-Ionyl)triphenylphosphonium Chloride

: 82848-18-8
1,12-Bis(2,6,6-trimethylcyclohex-1-enyl)-3,6,10-trimethyldodeca-1,3,5,7,9,11-hexaene

Guidance literature:: With potassium hydroxide; In methanol; Ambient temperature;
DOI:10.1021/jo00157a026

Reference yield:

: 7235-40-7
beta-carotene

: 85098-48-2
1,6-Bis(2,6,6-trimethylcyclohex-1-enyl)hexa-1,3,5-triene

: 85098-49-3
1,6-Bis(2,6,6-trimethylcyclohex-1-enyl)-3-methylhexa-1,3,5-triene

: 85098-47-1
1,12-Bis(2,6,6-trimethylcyclohex-1-enyl)-3,7-dimethyldodeca-1,3,5,7,9,11-hexaene

: 82848-18-8
1,12-Bis(2,6,6-trimethylcyclohex-1-enyl)-3,6,10-trimethyldodeca-1,3,5,7,9,11-hexaene

: 108-38-3,104809-90-7
m-xylene

: 108-88-3,15644-74-3,16713-13-6
toluene

Guidance literature:: at 145 ℃; Product distribution; var. solvents, var. temp.'s, var. reaction times;
DOI:10.1021/jo00157a026

Reference yield:

: 22029-76-1,27008-60-2,35031-11-9,53078-25-4,53108-96-6,81600-95-5,81801-17-4,83348-85-0,472-80-0
beta-ionol

: 82848-18-8
1,12-Bis(2,6,6-trimethylcyclohex-1-enyl)-3,6,10-trimethyldodeca-1,3,5,7,9,11-hexaene

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 6 h / Ambient temperature

2: HCl / methanol / 2 h / 35 °C

3: 55 percent / KOH / methanol / Ambient temperature

With hydrogenchloride; potassium hydroxide; In pyridine; methanol;
DOI:10.1021/jo00157a026