Technology Process of C18H28N2O3
There total 3 articles about C18H28N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
tert-butyl 3-oxoazetidine-1-carboxylate; 2-(2-methoxyphenyl)propan-2-amine;
With
acetic acid;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 3h;
Molecular sieve 4A;
With
sodium tris(acetoxy)borohydride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 3.5h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide / tetrahydrofuran / 1 h / 20 °C
2.1: triethylamine / sulfur trioxide pyridine complex / chloroform; dimethyl sulfoxide / 4 h / 20 °C
3.1: acetic acid / N,N-dimethyl-formamide / 3 h / 80 °C / Molecular sieve 4A
3.2: 3.5 h / 20 °C
With
acetic acid; triethylamine; sodium hydroxide;
sulfur trioxide pyridine complex;
In
tetrahydrofuran; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / sulfur trioxide pyridine complex / chloroform; dimethyl sulfoxide / 4 h / 20 °C
2.1: acetic acid / N,N-dimethyl-formamide / 3 h / 80 °C / Molecular sieve 4A
2.2: 3.5 h / 20 °C
With
acetic acid; triethylamine;
sulfur trioxide pyridine complex;
In
chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;