7-Chlor-3-(2-iodethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

Base Information

Chemical Name:7-Chlor-3-(2-iodethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin
CAS No.:86230-83-3
Molecular Formula:C₁₆H₁₃ClIN₃O
Molecular Weight:425.656
Hs Code.:

Synonyms:7-Chlor-3-(2-iodethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-Chlor-3-(2-iodethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

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Technology Process of 7-Chlor-3-(2-iodethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

There total 2 articles about 7-Chlor-3-(2-iodethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 86230-82-2
7-chloro-9-phenyl-1,2-dihydrooxazolo<2,3-b>-1,3,4-benzotriazepine

: 86230-83-3
7-Chlor-3-(2-iodethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

Guidance literature:: With hydrogen iodide; In 1,4-dioxane; water; for 48h; Ambient temperature;

Reference yield:

: 67862-90-2
7-chloro-3-(2-hydroxy-ethyl)-5-phenyl-1,3-dihydro-benzo[e][1,2,4]triazepine-2-thione

: 86230-83-3
7-Chlor-3-(2-iodethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaOCH₃ (1 mol/l), 30percent H₂O₂ / acetone; H₂O; methanol / 2 h / Ambient temperature

2: 80 percent / 43percent HI / dioxane; H₂O / 48 h / Ambient temperature

With hydrogen iodide; dihydrogen peroxide; sodium methylate; In 1,4-dioxane; methanol; water; acetone;