trifluoromethanesulfonic acid 1-(2-fluoro-phenyl)naphthalen-2-yl ester

Base Information

Chemical Name:trifluoromethanesulfonic acid 1-(2-fluoro-phenyl)naphthalen-2-yl ester
CAS No.:1264712-18-6
Molecular Formula:C₁₇H₁₀F₄O₃S
Molecular Weight:370.324
Hs Code.:

Synonyms:trifluoromethanesulfonic acid 1-(2-fluoro-phenyl)naphthalen-2-yl ester

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Chemical Property of trifluoromethanesulfonic acid 1-(2-fluoro-phenyl)naphthalen-2-yl ester

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Technology Process of trifluoromethanesulfonic acid 1-(2-fluoro-phenyl)naphthalen-2-yl ester

There total 1 articles about trifluoromethanesulfonic acid 1-(2-fluoro-phenyl)naphthalen-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1264712-17-5
1-(2-fluorophenyl)naphthalen-2-ol

: 1264712-18-6
trifluoromethanesulfonic acid 1-(2-fluoro-phenyl)naphthalen-2-yl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201001393

Reference yield: 93.0%

: 5466-06-8
3-mercaptopropionic acid ethyl ester

: 1264712-18-6
trifluoromethanesulfonic acid 1-(2-fluoro-phenyl)naphthalen-2-yl ester

: 1264712-19-7
3-[1-(2-fluorophenyl)naphthalen-2-ylsulfanyl]propionic acid ethyl ester

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether; In toluene; at 110 ℃; for 15h; Inert atmosphere;
DOI:10.1002/ejoc.201001393

Reference yield:

: 1264712-18-6
trifluoromethanesulfonic acid 1-(2-fluoro-phenyl)naphthalen-2-yl ester

: 205-43-6
Benzo[b]naphtho[1,2-d]thiophene

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 15 h / 110 °C / Inert atmosphere

2: potassium tert-butylate / tetrahydrofuran / 8 h / 50 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether; In tetrahydrofuran; toluene;
DOI:10.1002/ejoc.201001393