3-<<4-phenyl>thio>propionate

Base Information

Chemical Name:3-<<4-phenyl>thio>propionate
CAS No.:130198-87-7
Molecular Formula:C₁₄H₂₁NO₄S
Molecular Weight:299.391
Hs Code.:

3-<<4-<N,N-bis(2-hydroxyethyl)amino>phenyl>thio>propionate

Synonyms:3-<<4-phenyl>thio>propionate

Suppliers and Price of 3-<<4-phenyl>thio>propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<<4-phenyl>thio>propionate

Chemical Property:

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Technology Process of 3-<<4-phenyl>thio>propionate

There total 5 articles about 3-<<4-phenyl>thio>propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 3395-91-3
Methyl 3-bromopropionate

: 100132-31-8
4-benzenethiol

: 130198-87-7
3-<<4-phenyl>thio>propionate

Guidance literature:: With potassium carbonate; In methanol; for 0.166667h; Heating;
DOI:10.1021/jm00173a016

Reference yield:

: 130219-46-4
S-<(benzyloxy)carbonyl>-4-aminobenzenethiol

: 130198-87-7
3-<<4-phenyl>thio>propionate

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / AcOH / tetrahydrofuran / 336 h / 20 °C

2: 56 percent / NaOH / ethanol / 2 h / Heating

3: 57 percent / K₂CO₃ / methanol / 0.17 h / Heating

With sodium hydroxide; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/jm00173a016

Reference yield:

: 130198-85-5
S-<(benzyloxy)carbonyl>-4-nitrobenzenethiol

: 130198-87-7
3-<<4-phenyl>thio>propionate

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / SnCl₂*2H₂O / ethyl acetate / 4 h / Heating

2: 79 percent / AcOH / tetrahydrofuran / 336 h / 20 °C

3: 56 percent / NaOH / ethanol / 2 h / Heating

4: 57 percent / K₂CO₃ / methanol / 0.17 h / Heating

With sodium hydroxide; potassium carbonate; acetic acid; tin(ll) chloride; In tetrahydrofuran; methanol; ethanol; ethyl acetate;
DOI:10.1021/jm00173a016