Technology Process of C26H38N8O4
There total 7 articles about C26H38N8O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C29H42N8O4;
With
water; trifluoroacetic acid;
at 20 ℃;
for 1.5h;
In
methanol;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic acid / methanol / 20 °C / 4A MS
1.2: 1 h
2.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C
3.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 760.05 Torr
4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C
5.1: trifluoroacetic acid; water / 1.5 h / 20 °C
5.2: basic resin / 1 h
With
water; hydrogen; sodium tris(acetoxy)borohydride; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
palladium 10% on activated carbon;
In
methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C
2.1: hydrazine hydrate / ethanol / 3 h / 20 °C / Reflux
3.1: acetic acid / methanol / 20 °C / 4A MS
3.2: 1 h
4.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C
5.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 760.05 Torr
6.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C
7.1: trifluoroacetic acid; water / 1.5 h / 20 °C
7.2: basic resin / 1 h
With
water; hydrogen; sodium tris(acetoxy)borohydride; hydrazine hydrate; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;