tert-butyl (2S,3S,4E)-3-allyl<(1R)-1-phenylethyl>amino-2-hydroxy-4-hexenoate

Base Information

Chemical Name:tert-butyl (2S,3S,4E)-3-allyl<(1R)-1-phenylethyl>amino-2-hydroxy-4-hexenoate
CAS No.:198543-54-3
Molecular Formula:C₂₁H₃₁NO₃
Molecular Weight:345.482
Hs Code.:

Synonyms:tert-butyl (2S,3S,4E)-3-allyl<(1R)-1-phenylethyl>amino-2-hydroxy-4-hexenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (2S,3S,4E)-3-allyl<(1R)-1-phenylethyl>amino-2-hydroxy-4-hexenoate

Chemical Property:

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Technology Process of tert-butyl (2S,3S,4E)-3-allyl<(1R)-1-phenylethyl>amino-2-hydroxy-4-hexenoate

There total 3 articles about tert-butyl (2S,3S,4E)-3-allyl<(1R)-1-phenylethyl>amino-2-hydroxy-4-hexenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115914-08-4
(S)-N-(1-phenylethyl)prop-2-en-1-amine

: 81838-85-9
tert-butyl (2E,4E)-2,4-hexadienoate

: 198543-54-3
tert-butyl (2S,3S,4E)-3-allyl<(1R)-1-phenylethyl>amino-2-hydroxy-4-hexenoate

Guidance literature:: With n-butyllithium; (1S)-(+)-(10-camphorsulfonyl)-oxaziridine; Yield given; Multistep reaction; 1.) hexane, -78 deg C, 1 h, 2.) THF, -78 deg C, 1 h, 3.) -78 deg C, 6 h; warm to room temperature;
DOI:10.1016/S0040-4020(98)01051-5

Reference yield:

: 110-44-1,91751-55-2
sorbic Acid

: 198543-54-3
tert-butyl (2S,3S,4E)-3-allyl<(1R)-1-phenylethyl>amino-2-hydroxy-4-hexenoate

Guidance literature:: Multi-step reaction with 2 steps

1: conc. H₂SO₄

2: 2.) (+)-(camphorsulfonyl)oxaziridine / 1.) THF, -78 deg C, 1 h, 2.) THF

With (+)-(2S,8aS)-(camphorylsulfonyl)oxaziridine; sulfuric acid;
DOI:10.1016/S0957-4166(97)00470-9

Reference yield:

: 81838-85-9
tert-butyl (2E,4E)-2,4-hexadienoate

: lithium (S)-N-allyl-N-α-methylbenzyl amide

: 198543-54-3
tert-butyl (2S,3S,4E)-3-allyl<(1R)-1-phenylethyl>amino-2-hydroxy-4-hexenoate

Guidance literature:: With (+)-(2S,8aS)-(camphorylsulfonyl)oxaziridine; Yield given. Multistep reaction; 1.) THF, -78 deg C, 1 h, 2.) THF;
DOI:10.1016/S0957-4166(97)00470-9