2-imino-3-(2'-amino-4'-methoxyphenyl)-thiazolidine di(ethanesulfonate)

Base Information

Chemical Name:2-imino-3-(2'-amino-4'-methoxyphenyl)-thiazolidine di(ethanesulfonate)
CAS No.:100417-08-1
Molecular Formula:2C₂H₆O₃S*C₁₀H₁₃N₃OS
Molecular Weight:443.566
Hs Code.:

Synonyms:2-imino-3-(2'-amino-4'-methoxyphenyl)-thiazolidine di(ethanesulfonate)

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Chemical Property of 2-imino-3-(2'-amino-4'-methoxyphenyl)-thiazolidine di(ethanesulfonate)

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Technology Process of 2-imino-3-(2'-amino-4'-methoxyphenyl)-thiazolidine di(ethanesulfonate)

There total 4 articles about 2-imino-3-(2'-amino-4'-methoxyphenyl)-thiazolidine di(ethanesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100418-40-4
4-methoxy-2-nitro-N-(2-thiocyanatoethyl)-aniline

: 100417-08-1
2-imino-3-(2'-amino-4'-methoxyphenyl)-thiazolidine di(ethanesulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd-C / Ambient temperature; normal pressure

2: 0.25 h / 0 °C

With hydrogen; palladium on activated charcoal;
DOI:10.1016/S0040-4020(01)89768-4

Reference yield:

: 16036-42-3
N-(2-Bromoethyl)-4-methoxy-2-nitraniline

: 100417-08-1
2-imino-3-(2'-amino-4'-methoxyphenyl)-thiazolidine di(ethanesulfonate)

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / ethanol / 8 h / Heating

2: H₂ / 10percent Pd-C / Ambient temperature; normal pressure

3: 0.25 h / 0 °C

With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0040-4020(01)89768-4

Reference yield:

: 16058-88-1
N-(2-Bromoethyl)-N-tosyl-4-methoxy-2-nitraniline

: 100417-08-1
2-imino-3-(2'-amino-4'-methoxyphenyl)-thiazolidine di(ethanesulfonate)

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / conc. H₂SO₄ / 24 h / Ambient temperature

2: 89 percent / ethanol / 8 h / Heating

3: H₂ / 10percent Pd-C / Ambient temperature; normal pressure

4: 0.25 h / 0 °C

With sulfuric acid; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0040-4020(01)89768-4