C₃₄H₄₄N₂O₅SSi

Base Information

Chemical Name:C₃₄H₄₄N₂O₅SSi
CAS No.:1374109-04-2
Molecular Formula:C₃₄H₄₄N₂O₅SSi
Molecular Weight:620.885
Hs Code.:

C<sub>34</sub>H<sub>44</sub>N<sub>2</sub>O<sub>5</sub>SSi

Synonyms:C₃₄H₄₄N₂O₅SSi

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Chemical Property of C₃₄H₄₄N₂O₅SSi

Chemical Property:

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Technology Process of C₃₄H₄₄N₂O₅SSi

There total 5 articles about C₃₄H₄₄N₂O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70500-72-0
quinoline-2,7-diol

: 1374109-04-2
C₃₄H₄₄N₂O₅SSi

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride; N,N-dimethyl-formamide / 1 h / 20 - 70 °C / Cooling with ice

2: pyridinium p-toluenesulfonate / tetrahydrofuran / 16 h / 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 8 h / 80 °C / Inert atmosphere

4: trifluoroacetic acid / chloroform / 2 h / 20 °C / Cooling with ice

5: acetic acid; 2-picoline borane complex / methanol / 16 h / 20 °C / Cooling with ice

6: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18 h / 20 °C / Cooling with ice

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; 2-picoline borane complex; di-isopropyl azodicarboxylate; pyridinium p-toluenesulfonate; potassium carbonate; acetic acid; N,N-dimethyl-formamide; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; chloroform; water;

Reference yield:

: 375358-19-3
2-chloroquinoline-7-ol

: 1374109-04-2
C₃₄H₄₄N₂O₅SSi

Guidance literature:: Multi-step reaction with 5 steps

1: pyridinium p-toluenesulfonate / tetrahydrofuran / 16 h / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 8 h / 80 °C / Inert atmosphere

3: trifluoroacetic acid / chloroform / 2 h / 20 °C / Cooling with ice

4: acetic acid; 2-picoline borane complex / methanol / 16 h / 20 °C / Cooling with ice

5: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18 h / 20 °C / Cooling with ice

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-picoline borane complex; di-isopropyl azodicarboxylate; pyridinium p-toluenesulfonate; potassium carbonate; acetic acid; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; chloroform; water;

Reference yield:

: 1374108-60-7
C₁₃H₁₄ClNO₂

: 1374109-04-2
C₃₄H₄₄N₂O₅SSi

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 8 h / 80 °C / Inert atmosphere

2: trifluoroacetic acid / chloroform / 2 h / 20 °C / Cooling with ice

3: acetic acid; 2-picoline borane complex / methanol / 16 h / 20 °C / Cooling with ice

4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18 h / 20 °C / Cooling with ice

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-picoline borane complex; di-isopropyl azodicarboxylate; potassium carbonate; acetic acid; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; chloroform; water;