hexyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

Base Information

Chemical Name:hexyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate
CAS No.:1329454-64-9
Molecular Formula:C₂₇H₃₆O₁₄
Molecular Weight:584.574
Hs Code.:

Synonyms:hexyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hexyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

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Technology Process of hexyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

There total 3 articles about hexyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1329454-53-6
hexyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-O-isopropylidene-benzoate

: 1329454-64-9
hexyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2011.07.046

Reference yield:

: 1329454-45-6
C₁₆H₂₂O₅

: 1329454-64-9
hexyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane

2: trifluoroacetic acid / 24 h / 20 °C

With boron trifluoride diethyl etherate; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.tet.2011.07.046

Reference yield:

: 1087-26-9
n-hexyl gallate

: 1329454-64-9
hexyl 3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside)-4,5-dihydroxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: camphor-10-sulfonic acid / chloroform / 16 h / 60 °C

2: boron trifluoride diethyl etherate / dichloromethane

3: trifluoroacetic acid / 24 h / 20 °C

With camphor-10-sulfonic acid; boron trifluoride diethyl etherate; trifluoroacetic acid; In dichloromethane; chloroform;
DOI:10.1016/j.tet.2011.07.046