6-bromomethyl-2,3-diphenyl-5,6-dihydro-3H-[1,3]thiazolo[3,2-b][1,2,4]triazol-7-ium tribromide

Base Information

• Chemical Name: 6-bromomethyl-2,3-diphenyl-5,6-dihydro-3H-[1,3]thiazolo[3,2-b][1,2,4]triazol-7-ium tribromide
• CAS No.: 478789-45-6
• Molecular Formula: Br₃*C₁₇H₁₅BrN₃S
• Molecular Weight: 613.008

Synonyms:6-bromomethyl-2,3-diphenyl-5,6-dihydro-3H-[1,3]thiazolo[3,2-b][1,2,4]triazol-7-ium tribromide

Chemical Property of 6-bromomethyl-2,3-diphenyl-5,6-dihydro-3H-[1,3]thiazolo[3,2-b][1,2,4]triazol-7-ium tribromide

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Technology Process of 6-bromomethyl-2,3-diphenyl-5,6-dihydro-3H-[1,3]thiazolo[3,2-b][1,2,4]triazol-7-ium tribromide

There total 1 articles about 6-bromomethyl-2,3-diphenyl-5,6-dihydro-3H-[1,3]thiazolo[3,2-b][1,2,4]triazol-7-ium tribromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

3-allylsulfanyl-4,5-diphenyl-4H-[1,2,4]triazole (60738-42-3) → Br3(1-)*C17H15BrN3S(1+) + 6-bromomethyl-2,3-diphenyl-5,6-dihydro-3H-[1,3]thiazolo[3,2-b][1,2,4]triazol-7-ium tribromide (478789-45-6)

Guidance literature:

With bromine; for 4h; regioselective reaction; Cooling;

DOI:10.1007/s10593-011-0870-5

Reference yield: 85.0%

6-bromomethyl-2,3-diphenyl-5,6-dihydro-3H-[1,3]thiazolo[3,2-b][1,2,4]triazol-7-ium tribromide (478789-45-6) → 1-1-[2-(5-oxo-3,4-diphenyl-4,5-dihydro-1H-1,2,4-triazol-1-yl)allyldisulfanylmethyl]vinyl-3,4-diphenyl-4,5-dihydro-1H-1,2,4-triazol-5-one (1353875-35-0)

Guidance literature:

With sodium carbonate; In water; for 4h;

DOI:10.1007/s10593-011-0870-5

Reference yield: 84.0%

6-bromomethyl-2,3-diphenyl-5,6-dihydro-3H-[1,3]thiazolo[3,2-b][1,2,4]triazol-7-ium tribromide (478789-45-6) → 6-(bromomethyl)-2,3-diphenyl-5,6-dihydro-3H-[1,3]thiazolo[3,2-b][1,2,4]triazol-7-ium bromide

Guidance literature:

With acetone; at 20 ℃; for 1h;

DOI:10.1007/s10593-011-0870-5

upstream raw materials:

3-allylsulfanyl-4,5-diphenyl-4H-[1,2,4]triazole

Downstream raw materials:

1-1-[2-(5-oxo-3,4-diphenyl-4,5-dihydro-1H-1,2,4-triazol-1-yl)allyldisulfanylmethyl]vinyl-3,4-diphenyl-4,5-dihydro-1H-1,2,4-triazol-5-one

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