C₄₄H₂₆N₆O

Base Information

• Chemical Name: C₄₄H₂₆N₆O
• CAS No.: 1268851-63-3
• Molecular Formula: C₄₄H₂₆N₆O
• Molecular Weight: 654.73
• Mol file: 1268851-63-3.mol

Synonyms:C₄₄H₂₆N₆O

Chemical Property of C₄₄H₂₆N₆O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₄H₂₆N₆O

There total 6 articles about C₄₄H₂₆N₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

C44H28N6O → C44H26N6O (1268851-63-3)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1021/ol1031848

Reference yield:

meso-tetraphenylporphyrin-2,3-dione → C44H26N6O (1268851-63-3)

Guidance literature:

Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride / pyridine / 24 h / 20 °C / Inert atmosphere

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C

3: hydroxylamine hydrochloride / pyridine / 2 h / Inert atmosphere; Reflux

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C

With hydroxylamine hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In pyridine; dichloromethane;

DOI:10.1021/ol1031848

Reference yield:

C44H29N5O2 → C44H26N6O (1268851-63-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C

2: hydroxylamine hydrochloride / pyridine / 2 h / Inert atmosphere; Reflux

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C

With hydroxylamine hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In pyridine; dichloromethane;

DOI:10.1021/ol1031848

upstream raw materials:

C₄₄H₂₇N₅O₂

C₄₄H₂₇N₅O