N-(2-tert-butoxycarbonylamino-ethyl)-N-(3-chloro-phenyl)-oxalamic acid methyl ester

Base Information

• Chemical Name: N-(2-tert-butoxycarbonylamino-ethyl)-N-(3-chloro-phenyl)-oxalamic acid methyl ester
• CAS No.: 197913-10-3
• Molecular Formula: C₁₆H₂₁ClN₂O₅
• Molecular Weight: 356.806

Synonyms:N-(2-tert-butoxycarbonylamino-ethyl)-N-(3-chloro-phenyl)-oxalamic acid methyl ester

Chemical Property of N-(2-tert-butoxycarbonylamino-ethyl)-N-(3-chloro-phenyl)-oxalamic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of N-(2-tert-butoxycarbonylamino-ethyl)-N-(3-chloro-phenyl)-oxalamic acid methyl ester

There total 2 articles about N-(2-tert-butoxycarbonylamino-ethyl)-N-(3-chloro-phenyl)-oxalamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-chloroaniline hydrochloride (141-85-5) → N-(2-tert-butoxycarbonylamino-ethyl)-N-(3-chloro-phenyl)-oxalamic acid methyl ester (197913-10-3)

Guidance literature:

Multi-step reaction with 3 steps

1: various solvent(s) / 160 °C

2: aq. NaHCO₃ / tetrahydrofuran

3: 90 percent / aq. NaHCO₃ / ethyl acetate / 0 °C

With sodium hydrogencarbonate; In tetrahydrofuran; ethyl acetate;

DOI:10.1016/S0960-894X(00)00710-1

Reference yield:

N-(3-chlorophenyl)-1,2-diaminoethane (14088-83-6) → N-(2-tert-butoxycarbonylamino-ethyl)-N-(3-chloro-phenyl)-oxalamic acid methyl ester (197913-10-3)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaHCO₃ / tetrahydrofuran

2: 90 percent / aq. NaHCO₃ / ethyl acetate / 0 °C

With sodium hydrogencarbonate; In tetrahydrofuran; ethyl acetate;

DOI:10.1016/S0960-894X(00)00710-1

Reference yield: 100.0%

N-(2-tert-butoxycarbonylamino-ethyl)-N-(3-chloro-phenyl)-oxalamic acid methyl ester (197913-10-3) → N-(2-amino-ethyl)-N-(3-chloro-phenyl)-oxalamic acid methyl ester; hydrochloride

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 0 ℃;

DOI:10.1016/S0960-894X(00)00710-1

upstream raw materials:

3-chloroaniline hydrochloride

N-(3-chlorophenyl)-1,2-diaminoethane

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