Thiophosphorsaeure-O-(4-chlor-2-methyl-6-phenylpyrimidin-5-yl)-O,O-diethylester

Base Information

Chemical Name:Thiophosphorsaeure-O-(4-chlor-2-methyl-6-phenylpyrimidin-5-yl)-O,O-diethylester
CAS No.:120456-81-7
Molecular Formula:C₁₅H₁₈ClN₂O₃PS
Molecular Weight:372.812
Hs Code.:

Synonyms:Thiophosphorsaeure-O-(4-chlor-2-methyl-6-phenylpyrimidin-5-yl)-O,O-diethylester

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Chemical Property of Thiophosphorsaeure-O-(4-chlor-2-methyl-6-phenylpyrimidin-5-yl)-O,O-diethylester

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Technology Process of Thiophosphorsaeure-O-(4-chlor-2-methyl-6-phenylpyrimidin-5-yl)-O,O-diethylester

There total 4 articles about Thiophosphorsaeure-O-(4-chlor-2-methyl-6-phenylpyrimidin-5-yl)-O,O-diethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 2524-04-1
diethyl phosphorochloridothioate

: 120456-63-5
4-Chlor-5-hydroxy-2-methyl-6-phenylpyrimidin

: 120456-81-7
Thiophosphorsaeure-O-(4-chlor-2-methyl-6-phenylpyrimidin-5-yl)-O,O-diethylester

Guidance literature:: With triethylamine; In diethyl ether; Heating;
DOI:10.1007/BF00810105

Reference yield:

: 120456-48-6
5-Benzyloxy-2-methyl-4-phenyl-1H-pyrimidin-6-on

: 120456-81-7
Thiophosphorsaeure-O-(4-chlor-2-methyl-6-phenylpyrimidin-5-yl)-O,O-diethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / POCl₃ / 1 h / Heating

2: 55 percent / H₂ / 5percent Pd/C / ethyl acetate / 1 h

3: 83 percent / NEt₃ / diethyl ether / Heating

With hydrogen; triethylamine; trichlorophosphate; palladium on activated charcoal; In diethyl ether; ethyl acetate;
DOI:10.1007/BF00810105

Reference yield:

: 120456-58-8
5-Benzyloxy-4-chlor-2-methyl-6-phenylpyrimidin

: 120456-81-7
Thiophosphorsaeure-O-(4-chlor-2-methyl-6-phenylpyrimidin-5-yl)-O,O-diethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / H₂ / 5percent Pd/C / ethyl acetate / 1 h

2: 83 percent / NEt₃ / diethyl ether / Heating

With hydrogen; triethylamine; palladium on activated charcoal; In diethyl ether; ethyl acetate;
DOI:10.1007/BF00810105