C₁₅H₁₄BrN

Base Information

• Chemical Name: C₁₅H₁₄BrN
• CAS No.: 405288-81-5
• Molecular Formula: C₁₅H₁₄BrN
• Molecular Weight: 288.187

Synonyms:C₁₅H₁₄BrN

Chemical Property of C₁₅H₁₄BrN

Chemical Property:

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Technology Process of C₁₅H₁₄BrN

There total 1 articles about C₁₅H₁₄BrN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bromo-benzaldehyde (1122-91-4) + 2,4-Xylidine (95-68-1) → C15H14BrN (405288-81-5)

Guidance literature:

In ethanol; for 3h; Reflux;

DOI:10.1002/chem.201103562

Reference yield: 80.0%

(E)-1,1-dimethyl-2-(2-methylallylidene)hydrazine (66064-57-1) + C15H14BrN (405288-81-5) → 4-bromobenzaldehyde N,N-dimethylhydrazone (32787-75-0) + (+/-)-(2S*,4S*)-2-(4-bromophenyl)-4-[(2,2-dimethylhydrazono)methyl]-4,6,8-trimethyl-1,2,3,4-tetrahydroquinoline

Guidance literature:

With indium(III) chloride; In acetonitrile; at 20 ℃; for 3h; diastereoselective reaction;

DOI:10.1002/chem.201103562

upstream raw materials:

4-bromo-benzaldehyde

2,4-Xylidine

Downstream raw materials:

4-bromobenzaldehyde N,N-dimethylhydrazone

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