[4-(2,6-dimethoxypyrimidin-4-yl)cyclohex-2-ene-1,1-diyl]bis(methylene) dibenzoate

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Chemical Name:[4-(2,6-dimethoxypyrimidin-4-yl)cyclohex-2-ene-1,1-diyl]bis(methylene) dibenzoate
CAS No.:1269417-36-8
Molecular Formula:C₂₈H₂₈N₂O₆
Molecular Weight:488.54
Hs Code.:

Synonyms:[4-(2,6-dimethoxypyrimidin-4-yl)cyclohex-2-ene-1,1-diyl]bis(methylene) dibenzoate

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Chemical Property of [4-(2,6-dimethoxypyrimidin-4-yl)cyclohex-2-ene-1,1-diyl]bis(methylene) dibenzoate

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Technology Process of [4-(2,6-dimethoxypyrimidin-4-yl)cyclohex-2-ene-1,1-diyl]bis(methylene) dibenzoate

There total 2 articles about [4-(2,6-dimethoxypyrimidin-4-yl)cyclohex-2-ene-1,1-diyl]bis(methylene) dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1269417-37-9
(4-chlorocyclohex-2-ene-1,1-diyl)bis(methylene) dibenzoate

: 69696-44-2
6-iodo-2,4-dimethoxypyrimidine

: 1269417-36-8
[4-(2,6-dimethoxypyrimidin-4-yl)cyclohex-2-ene-1,1-diyl]bis(methylene) dibenzoate

Guidance literature:: 6-iodo-2,4-dimethoxypyrimidine; With TurboGrignard; In tetrahydrofuran; at -25 ℃; for 1h; Inert atmosphere;

(4-chlorocyclohex-2-ene-1,1-diyl)bis(methylene) dibenzoate; With copper(l) iodide; lithium chloride; In tetrahydrofuran; at -25 ℃; for 48h; Inert atmosphere;
DOI:10.1055/s-0030-1258271

Reference yield: 33.0%

: 1269417-62-0
(4-iodocyclohex-2-ene-1,1-diyl)bis(methylene) dibenzoate

: 69696-44-2
6-iodo-2,4-dimethoxypyrimidine

: 1269417-36-8
[4-(2,6-dimethoxypyrimidin-4-yl)cyclohex-2-ene-1,1-diyl]bis(methylene) dibenzoate

Guidance literature:: 6-iodo-2,4-dimethoxypyrimidine; With TurboGrignard; In tetrahydrofuran; at -25 ℃; for 1h; Inert atmosphere;

(4-iodocyclohex-2-ene-1,1-diyl)bis(methylene) dibenzoate; With copper(l) iodide; lithium chloride; In tetrahydrofuran; at -25 - 20 ℃; for 17h; Inert atmosphere;
DOI:10.1055/s-0030-1258271