PdCl₂(C₅H₅N)(P(C₆H₅)3)

Base Information

Chemical Name:PdCl₂(C₅H₅N)(P(C₆H₅)3)
CAS No.:88227-30-9
Molecular Formula:C₂₃H₂₀Cl₂NPPd
Molecular Weight:518.718
Hs Code.:

PdCl<sub>2</sub>(C<sub>5</sub>H<sub>5</sub>N)(P(C<sub>6</sub>H<sub>5</sub>)3)

Synonyms:PdCl₂(C₅H₅N)(P(C₆H₅)3)

Suppliers and Price of PdCl₂(C₅H₅N)(P(C₆H₅)3)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of PdCl₂(C₅H₅N)(P(C₆H₅)3)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of PdCl₂(C₅H₅N)(P(C₆H₅)3)

There total 1 articles about PdCl₂(C₅H₅N)(P(C₆H₅)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: trans(P,N)-bis(μ-pyridyl-C(2),N)-bis{chloro(triphenylphosphine)palladium(II)}

: 88227-30-9
PdCl₂(C₅H₅N)(P(C₆H₅)3)

Guidance literature:: With hydrogenchloride; In methanol; dichloromethane; a CH2Cl2 soln. of Pd2 complex was treated with methanolic HCl (molar ratio Pd/HCl 1/3) at room temp., the mixt. was set aside overnight; ppt. was filtered off, Et2O was added to the concd. filtrate to give a second crop of the product; elem. anal.;
DOI:10.1016/S0022-328X(00)98785-0

Reference yield: 83.0%

: 88227-30-9
PdCl₂(C₅H₅N)(P(C₆H₅)3)

: (PdCl(NC₅H₅)(P(C₆H₅)3)2)⁽¹⁺⁾*ClO₄^(1-)=(PdCl(NC₅H₅)(P(C₆H₅)3)2)ClO₄

Guidance literature:: With PPh₃; NaClO₄; In methanol; dichloromethane; a suspn. of cis-(PdCl2(2-pyH)(PPh3)) in CH2Cl2 is treated with PPh3, mixt. stirred until complete dissoln., methanolic soln. NaClO4*H2O added;; after 5 min solvents evapd. to dryness, solid residue extd. with CH2Cl2in the presence of charcoal, ext. filtered and concd., Et2O added; elem. anal.;;
DOI:10.1016/S0020-1693(00)87650-1

Reference yield: 82.0%

: 88227-30-9
PdCl₂(C₅H₅N)(P(C₆H₅)3)

: 593-75-9,685498-28-6
methyl isocyanate

: (Pd(NC₅H₅)(CNCH₃)(P(C₆H₅)3)2)⁽²⁺⁾*2ClO₄^(1-)=(Pd(NC₅H₅)(CNCH₃)(P(C₆H₅)3)2)(ClO₄)2

Guidance literature:: With PPh₃; NaClO₄; In methanol; dichloromethane; a suspn. of cis-(PdCl2(2-pyH)(PPh3)) in CH2Cl2 is treated with PPh3 under stirring, NaClO4*H2O in methanol and isocyanide in CH2Cl2 successively added;; solvents evapd. to dryness, residue extd. with CH2Cl2 in the presence of charcoal, ext. filtered and concd., CH2Cl2/Et2O added; elem. anal.;
DOI:10.1016/S0020-1693(00)87650-1