(3-(4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazin-2-yl)phenyl)(1-trityl-1H-imidazol-4-yl)methanol

Base Information

• Chemical Name: (3-(4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazin-2-yl)phenyl)(1-trityl-1H-imidazol-4-yl)methanol
• CAS No.: 1029690-56-9
• Molecular Formula: C₃₆H₃₅N₃O₂
• Molecular Weight: 541.693

Synonyms:(3-(4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazin-2-yl)phenyl)(1-trityl-1H-imidazol-4-yl)methanol

Chemical Property of (3-(4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazin-2-yl)phenyl)(1-trityl-1H-imidazol-4-yl)methanol

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Technology Process of (3-(4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazin-2-yl)phenyl)(1-trityl-1H-imidazol-4-yl)methanol

There total 1 articles about (3-(4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazin-2-yl)phenyl)(1-trityl-1H-imidazol-4-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1-tritylimidazol-4-yl)carboxaldehyde (33016-47-6) + 2-(3-bromophenyl)-4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazine (24314-25-8) → (3-(4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazin-2-yl)phenyl)(1-trityl-1H-imidazol-4-yl)methanol (1029690-56-9)

Guidance literature:

2-(3-bromophenyl)-4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazine; With magnesium; In tetrahydrofuran; at 66 ℃; for 0.5h;

(1-tritylimidazol-4-yl)carboxaldehyde; In tetrahydrofuran; at 20 ℃; for 1.5h;

DOI:10.1021/jm7014149

Reference yield: 65.0%

(3-(4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazin-2-yl)phenyl)(1-trityl-1H-imidazol-4-yl)methanol (1029690-56-9) → 2-(3-((1H-imidazol-4-yl)methyl)phenyl)-4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazine (1029690-43-4)

Guidance literature:

With 10% Pd/C; hydrogen; acetic acid; at 60 ℃; for 4h; under 6981.68 Torr;

DOI:10.1021/jm7014149

upstream raw materials:

(1-tritylimidazol-4-yl)carboxaldehyde

2-(3-bromophenyl)-4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazine

Downstream raw materials:

2-(3-((1H-imidazol-4-yl)methyl)phenyl)-4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazine

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