(1aR,1bS,5aS,6R,6aS)-3-Benzyl-1a-methyl-octahydro-1-oxa-3-aza-cyclopropa[a]indene-5a,6-diol

Base Information

• Chemical Name: (1aR,1bS,5aS,6R,6aS)-3-Benzyl-1a-methyl-octahydro-1-oxa-3-aza-cyclopropa[a]indene-5a,6-diol
• CAS No.: 196859-91-3
• Molecular Formula: C₁₆H₂₁NO₃
• Molecular Weight: 275.348

Synonyms:(1aR,1bS,5aS,6R,6aS)-3-Benzyl-1a-methyl-octahydro-1-oxa-3-aza-cyclopropa[a]indene-5a,6-diol

Chemical Property of (1aR,1bS,5aS,6R,6aS)-3-Benzyl-1a-methyl-octahydro-1-oxa-3-aza-cyclopropa[a]indene-5a,6-diol

Chemical Property:

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Technology Process of (1aR,1bS,5aS,6R,6aS)-3-Benzyl-1a-methyl-octahydro-1-oxa-3-aza-cyclopropa[a]indene-5a,6-diol

There total 1 articles about (1aR,1bS,5aS,6R,6aS)-3-Benzyl-1a-methyl-octahydro-1-oxa-3-aza-cyclopropa[a]indene-5a,6-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzylamine hydrochloride (3287-99-8,39110-74-2,108321-65-9) + (1aR,1bS,5aS,6R,6aS)-1a-Methyl-1b,2,6,6a-tetrahydro-1aH-1,3-dioxa-cyclopropa[a]indene-2,5a,6-triol → (1aR,1bS,5aS,6R,6aS)-3-Benzyl-1a-methyl-octahydro-1-oxa-3-aza-cyclopropa[a]indene-5a,6-diol (196859-91-3)

Guidance literature:

With sodium cyanoborohydride; Yield given. Multistep reaction; 1.) MeOH, RT, 3 h, 2.) MeOH, 3 d;

DOI:10.1021/np9702648

Reference yield: 89.0%

(1aR,1bS,5aS,6R,6aS)-3-Benzyl-1a-methyl-octahydro-1-oxa-3-aza-cyclopropa[a]indene-5a,6-diol (196859-91-3) → (4aS,5R,6R,7R,7aR)-6-Azido-2-benzyl-7-methyl-octahydro-[2]pyrindine-4a,5,7-triol

Guidance literature:

With sodium azide; ammonium chloride; In methanol; water; at 80 ℃; for 21h;

DOI:10.1021/np9702648

Reference yield: 83.0%

(1aR,1bS,5aS,6R,6aS)-3-Benzyl-1a-methyl-octahydro-1-oxa-3-aza-cyclopropa[a]indene-5a,6-diol (196859-91-3) → (1aR,1bS,5aS,6R,6aS)-1a-Methyl-octahydro-1-oxa-3-aza-cyclopropa[a]indene-5a,6-diol

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1021/np9702648

upstream raw materials:

benzylamine hydrochloride

Downstream raw materials:

(4aS,5R,7S,7aR)-2-Benzyl-7-methyl-octahydro-[2]pyrindine-4a,5,7-triol

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