{Cp*Re(CO)(PMe₃)(p-N₂C₆H₄OMe)}{BF₄}

Base Information

Chemical Name:{Cp*Re(CO)(PMe₃)(p-N₂C₆H₄OMe)}{BF₄}
CAS No.:101835-38-5
Molecular Formula:BF₄*C₂₁H₃₁N₂O₂PRe
Molecular Weight:647.475
Hs Code.:

{Cp*Re(CO)(PMe<sub>3</sub>)(p-N<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OMe)}{BF<sub>4</sub>}

Synonyms:{Cp*Re(CO)(PMe₃)(p-N₂C₆H₄OMe)}{BF₄}

Suppliers and Price of {Cp*Re(CO)(PMe₃)(p-N₂C₆H₄OMe)}{BF₄}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {Cp*Re(CO)(PMe₃)(p-N₂C₆H₄OMe)}{BF₄}

Chemical Property:

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Technology Process of {Cp*Re(CO)(PMe₃)(p-N₂C₆H₄OMe)}{BF₄}

There total 1 articles about {Cp*Re(CO)(PMe₃)(p-N₂C₆H₄OMe)}{BF₄} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 94405-88-6
{Cp*Re(CO)(NCMe)(p-N₂C₆H₄OMe)}{BF₄}

: 594-09-2
trimethylphosphane

: 101835-38-5
{Cp*Re(CO)(PMe₃)(p-N₂C₆H₄OMe)}{BF₄}

Guidance literature:: In acetone; under N2, stirred, IR-control, ca. 4 h, room temp.; evapn., washed (diethyl ether), evapn. (2 d); elem. anal.;

Reference yield: 78.0%

: 101835-38-5
{Cp*Re(CO)(PMe₃)(p-N₂C₆H₄OMe)}{BF₄}

: potassium chloride

: ((CH₃)5C₅)Re(Cl)(P(CH₃)3)(N₂C₆H₄OCH₃)

Guidance literature:: With sodium hydroxide; In ethanol; chloroform; stirring (overnight); filtering, evapn. (vac.), extg. (hexane), evapn., recrystn. (hexane); elem. anal.;
DOI:10.1021/om950578v

Reference yield: 51.0%

: 101835-38-5
{Cp*Re(CO)(PMe₃)(p-N₂C₆H₄OMe)}{BF₄}

: 101835-36-3
(η5-C5Me5)Re(CO)(PMe3)N2

: Cp*Re(CO)(PMe₃)(p-NN(t-Bu)C₆H₄OMe)

Guidance literature:: With t-butyllithium or n-butyllithium; In tetrahydrofuran; under N2, Re-complex in THF heated (60°C), addn. of excess of t-butyllithium, color change from orange-red to light brown, stirred (15 min., room temp.), volume reduced under vacuum; water added (to hydrolyze unreacted t-butyllithium), stirred (5 min), addn. of ether, stirred (15 min), filtration (short column Celite-neutral alumina), evapn., chromy., recrystn. (n-pentane, -78°C); elem. anal.;