3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-glutaric acid monoester

Base Information

Chemical Name:3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-glutaric acid monoester
CAS No.:470480-98-9
Molecular Formula:C₂₈H₂₇N₃O₆
Molecular Weight:501.539
Hs Code.:

Synonyms:3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-glutaric acid monoester

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Chemical Property of 3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-glutaric acid monoester

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Technology Process of 3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-glutaric acid monoester

There total 1 articles about 3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-glutaric acid monoester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 108-55-4
glutaric anhydride,

: 237766-09-5
[3-(acridin-9-ylamino)-5-hydroxymethylphenyl]carbamic acidethyl ester

: 470480-98-9
3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-glutaric acid monoester

Guidance literature:: With pyridine; dmap; at 85 - 90 ℃; for 12h;
DOI:10.1021/jm0200714

Reference yield: 78.0%

: 155791-66-5
N-[2-(dimethylamino)ethyl]-1-methyl-4-aminopyrrolo-2-carboxamide

: 470480-98-9
3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-glutaric acid monoester

: 4-[5-(2-dimethylamino-ethylcarbamoyl)-1-methyl-1H-pyrrol-3-ylcarbamoyl]-butyric acid 3-(acridin-9-ylamino)-5-ethoxycarbonylamino-benzyl ester

Guidance literature:: 3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-glutaric acid monoester; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; at -5 ℃; for 2h;

N-[2-(dimethylamino)ethyl]-1-methyl-4-aminopyrrolo-2-carboxamide; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1021/jm0200714

Reference yield: 50.8%

: 162934-64-7
C₁₆H₂₄N₆O₂

: 470480-98-9
3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-glutaric acid monoester

: N-[2-(dimethylamino)ethyl]-1-methyl-4-[1-methyl-4-[[[3-(9-acridinylamino)-5-(ethoxycarbonylamino)benzyloxy]carbonylbutanoyl]amino]pyrrole-2-carboxamido]pyrrole-2-carboxamide

Guidance literature:: 3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-glutaric acid monoester; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; at -5 ℃; for 2h;

C₁₆H₂₄N₆O₂; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1021/jm0200714