5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphinatozinc

Base Information

Chemical Name:5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphinatozinc
CAS No.:253199-37-0
Molecular Formula:C₄₄H₁₇Cl₆F₅N₄Zn
Molecular Weight:974.746
Hs Code.:

Synonyms:5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphinatozinc

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphinatozinc

Chemical Property:

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Technology Process of 5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphinatozinc

There total 1 articles about 5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphinatozinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)-21H,23H-porphyrin

: 5970-45-6
zinc(II) acetate dihydrate

: 253199-37-0
5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphinatozinc

Guidance literature:: In methanol; dichloromethane; (Ar); heating (reflux, 12 h); cooling (room temp.), vac. evapn., addn. of CH2Cl2, washing (H2O, brine), drying (Na2SO4), filtn., vac. evapn., recrystn. (CH2Cl2/hexane); elem.anal.;
DOI:10.1021/jp991766s

Reference yield: 97.0%

: 253199-37-0
5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphinatozinc

: 111-33-1
1,3-bis(methylamino)propane

: 253199-43-8
(CH₃NH(CH₂)3NCH₃F₄C₆)(Cl₂C₆H₃)3C₂₀H₈N₄Zn

Guidance literature:: In neat (no solvent); (Ar); stirring (135°C, 2 h); cooling (room temp.), addn. of CH2Cl2, washing (NH4Cl soln., H2O, brine), drying (MgSO4) filtn., vac. evapn., recrystn. (CHCl3/hexane); elem. anal.;
DOI:10.1021/jp991766s

Reference yield: 54.0%

: 253199-37-0
5-(pentafluorophenyl)-10,15,20-tris(2,6-dichlorophenyl)porphinatozinc

: 253199-43-8
(CH₃NH(CH₂)3NCH₃F₄C₆)(Cl₂C₆H₃)3C₂₀H₈N₄Zn

: 253199-51-8
ZnC₂₀H₈N₄(Cl₂C₆H₃)3(C₆F₄CH₃N(CH₂)3NCH₃F₄C₆)(Cl₂C₆H₃)3C₂₀H₈N₄Zn

Guidance literature:: With tributyl-amine; In dimethyl sulfoxide; (Ar); stirring (130°C, 10 h); cooling (room temp.), addn. of CH2Cl2, washing (aq. NH4Cl, brine), drying (MgSO4), vac. evapn., chromy. (SiO2, petroleum ether/CH2Cl2);
DOI:10.1021/jp991766s