3,4,5-Tris-(2-{2-[2-(2-chloro-acetylamino)-ethoxy]-ethoxy}-ethoxy)-benzoic acid methyl ester

Base Information

Chemical Name:3,4,5-Tris-(2-{2-[2-(2-chloro-acetylamino)-ethoxy]-ethoxy}-ethoxy)-benzoic acid methyl ester
CAS No.:202803-53-0
Molecular Formula:C₃₂H₅₀Cl₃N₃O₁₄
Molecular Weight:807.12
Hs Code.:

Synonyms:3,4,5-Tris-(2-{2-[2-(2-chloro-acetylamino)-ethoxy]-ethoxy}-ethoxy)-benzoic acid methyl ester

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Chemical Property of 3,4,5-Tris-(2-{2-[2-(2-chloro-acetylamino)-ethoxy]-ethoxy}-ethoxy)-benzoic acid methyl ester

Chemical Property:

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Technology Process of 3,4,5-Tris-(2-{2-[2-(2-chloro-acetylamino)-ethoxy]-ethoxy}-ethoxy)-benzoic acid methyl ester

There total 8 articles about 3,4,5-Tris-(2-{2-[2-(2-chloro-acetylamino)-ethoxy]-ethoxy}-ethoxy)-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 541-88-8
Chloroacetic anhydride

: 202803-50-7
3,4,5-Tris-{2-[2-(2-amino-ethoxy)-ethoxy]-ethoxy}-benzoic acid methyl ester

: 202803-53-0
3,4,5-Tris-(2-{2-[2-(2-chloro-acetylamino)-ethoxy]-ethoxy}-ethoxy)-benzoic acid methyl ester

Guidance literature:: With triethylamine; In ethanol; for 2h; Ambient temperature;
DOI:10.1139/v97-177

Reference yield:

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 202803-53-0
3,4,5-Tris-(2-{2-[2-(2-chloro-acetylamino)-ethoxy]-ethoxy}-ethoxy)-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 44 percent / NaN₃ / ethanol / 4 h / Heating

2: 65 percent / K₂CO₃ / dimethylformamide / 24 h / 80 °C

3: H₂ / 10percent Pd/C / ethanol / 3 h / Ambient temperature

4: 65 percent / Et₃N / ethanol / 2 h / Ambient temperature

With sodium azide; hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1139/v97-177

Reference yield:

: 149-91-7
3,4,5-trihydroxybenzoic acid

: 202803-53-0
3,4,5-Tris-(2-{2-[2-(2-chloro-acetylamino)-ethoxy]-ethoxy}-ethoxy)-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: SOCl₂ / 2 h / Ambient temperature

2: 0.5 h

3: 65 percent / K₂CO₃ / dimethylformamide / 24 h / 80 °C

4: H₂ / 10percent Pd/C / ethanol / 3 h / Ambient temperature

5: 65 percent / Et₃N / ethanol / 2 h / Ambient temperature

With thionyl chloride; hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1139/v97-177