1-((4-(hydroxymethyl)cyclohexyl)methoxy)-5-(methoxymethyl)-2,3,4,6-tetramethylbenzene

Base Information

Chemical Name:1-((4-(hydroxymethyl)cyclohexyl)methoxy)-5-(methoxymethyl)-2,3,4,6-tetramethylbenzene
CAS No.:865625-97-4
Molecular Formula:C₂₀H₃₂O₃
Molecular Weight:320.472
Hs Code.:

Synonyms:1-((4-(hydroxymethyl)cyclohexyl)methoxy)-5-(methoxymethyl)-2,3,4,6-tetramethylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-((4-(hydroxymethyl)cyclohexyl)methoxy)-5-(methoxymethyl)-2,3,4,6-tetramethylbenzene

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Technology Process of 1-((4-(hydroxymethyl)cyclohexyl)methoxy)-5-(methoxymethyl)-2,3,4,6-tetramethylbenzene

There total 5 articles about 1-((4-(hydroxymethyl)cyclohexyl)methoxy)-5-(methoxymethyl)-2,3,4,6-tetramethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 865625-95-2
5-(methoxymethyl)-2,3,4,6-tetramethylphenol

: 137384-55-5
(4-bromomethylcyclohexane-1-yl)-methanol

: 865625-97-4
1-((4-(hydroxymethyl)cyclohexyl)methoxy)-5-(methoxymethyl)-2,3,4,6-tetramethylbenzene

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile; for 72h; Heating;
DOI:10.1021/ma0508146

Reference yield:

: C₁₁H₁₅BrO

: 865625-97-4
1-((4-(hydroxymethyl)cyclohexyl)methoxy)-5-(methoxymethyl)-2,3,4,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / methanol / 13 h / Heating

2: 91 percent / K₂CO₃ / KI / acetonitrile / 72 h / Heating

With potassium carbonate; potassium iodide; In methanol; acetonitrile;
DOI:10.1021/ma0508146

Reference yield:

: 527-60-6
Mesitol

: 865625-97-4
1-((4-(hydroxymethyl)cyclohexyl)methoxy)-5-(methoxymethyl)-2,3,4,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / NaBr; acetic acid; H₂SO₄ / 1 h / 20 °C

2: 77 percent / LiAlH₄ / diethyl ether / 0.5 h / 20 °C

3: NaBr; acetic acid; H₂SO₄ / 12 h / 20 °C

4: 57 percent / methanol / 13 h / Heating

5: 91 percent / K₂CO₃ / KI / acetonitrile / 72 h / Heating

With lithium aluminium tetrahydride; sulfuric acid; potassium carbonate; acetic acid; sodium bromide; potassium iodide; In methanol; diethyl ether; acetonitrile;
DOI:10.1021/ma0508146