benzyl (4S)-4-{[N-2-(tert-butoxycarbonyl)-L-asparaginyl]amino}-3-oxopentanoate

Base Information

Chemical Name:benzyl (4S)-4-{[N-2-(tert-butoxycarbonyl)-L-asparaginyl]amino}-3-oxopentanoate
CAS No.:1094530-61-6
Molecular Formula:C₂₁H₂₉N₃O₇
Molecular Weight:435.477
Hs Code.:

Synonyms:benzyl (4S)-4-{[N-2-(tert-butoxycarbonyl)-L-asparaginyl]amino}-3-oxopentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (4S)-4-{[N-2-(tert-butoxycarbonyl)-L-asparaginyl]amino}-3-oxopentanoate

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Technology Process of benzyl (4S)-4-{[N-2-(tert-butoxycarbonyl)-L-asparaginyl]amino}-3-oxopentanoate

There total 1 articles about benzyl (4S)-4-{[N-2-(tert-butoxycarbonyl)-L-asparaginyl]amino}-3-oxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 40204-26-0
malonic acid monobenzyl ester

: 56357-42-7
N-2-(tert-butoxycarbonyl)-L-asparaginyl-L-alanine

: 1094530-61-6
benzyl (4S)-4-{[N-2-(tert-butoxycarbonyl)-L-asparaginyl]amino}-3-oxopentanoate

Guidance literature:: N-2-(tert-butoxycarbonyl)-L-asparaginyl-L-alanine; With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; for 0.25h;

malonic acid monobenzyl ester; With dibutylmagnesium; In tetrahydrofuran; hexane; at 0 - 20 ℃;

In tetrahydrofuran; hexane; N,N-dimethyl-formamide; for 8h;
DOI:10.1021/jo801993k

Reference yield: 64.0%

: 75-11-6
diiodomethane

: 1094530-61-6
benzyl (4S)-4-{[N-2-(tert-butoxycarbonyl)-L-asparaginyl]amino}-3-oxopentanoate

: 1137728-52-9
benzyl (5S)-5-{[N-2-(tert-butoxycarbonyl)-L-asparaginyl]amino}-4-oxohexanoate

Guidance literature:: diiodomethane; With diethylzinc; In hexane; dichloromethane; at 0 ℃;

benzyl (4S)-4-{[N-2-(tert-butoxycarbonyl)-L-asparaginyl]amino}-3-oxopentanoate; In hexane; dichloromethane; for 0.0333333h;
DOI:10.1021/jo801993k