S-phenyl 2-O-benzyl-3,5-O-(di-tert-butylsilylene)-1-thio-α-L-arabinofuranoside S-oxide

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Chemical Name:S-phenyl 2-O-benzyl-3,5-O-(di-tert-butylsilylene)-1-thio-α-L-arabinofuranoside S-oxide
CAS No.:932719-30-7
Molecular Formula:C₂₆H₃₆O₅SSi
Molecular Weight:488.72
Hs Code.:

Synonyms:S-phenyl 2-O-benzyl-3,5-O-(di-tert-butylsilylene)-1-thio-α-L-arabinofuranoside S-oxide

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Chemical Property of S-phenyl 2-O-benzyl-3,5-O-(di-tert-butylsilylene)-1-thio-α-L-arabinofuranoside S-oxide

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Technology Process of S-phenyl 2-O-benzyl-3,5-O-(di-tert-butylsilylene)-1-thio-α-L-arabinofuranoside S-oxide

There total 3 articles about S-phenyl 2-O-benzyl-3,5-O-(di-tert-butylsilylene)-1-thio-α-L-arabinofuranoside S-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 913060-79-4
S-phenyl 2-O-benzyl-3,5-O-(di-tert-butylsilylene)-1-thio-α-L-arabinofuranoside

: 932719-30-7
S-phenyl 2-O-benzyl-3,5-O-(di-tert-butylsilylene)-1-thio-α-L-arabinofuranoside S-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 20 ℃; for 1h;
DOI:10.1021/jo061440x

Reference yield:

: trifluoro-methanesulfonic acid 7-benzyloxy-2,2-di-tert-butyl-tetrahydro-furo[3,2-d][1,3,2]dioxasilin-6-yl ester

: 932719-30-7
S-phenyl 2-O-benzyl-3,5-O-(di-tert-butylsilylene)-1-thio-α-L-arabinofuranoside S-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / -78 - -30 °C

2: 79 percent / meta-chloroperbenzoic acid / CH₂Cl₂ / 1 h / -78 - 20 °C

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo061440x

Reference yield:

: 108-98-5
thiophenol

: 932719-30-7
S-phenyl 2-O-benzyl-3,5-O-(di-tert-butylsilylene)-1-thio-α-L-arabinofuranoside S-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / -78 - -30 °C

2: 79 percent / meta-chloroperbenzoic acid / CH₂Cl₂ / 1 h / -78 - 20 °C

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo061440x