C₁₅H₂₀O₄

Base Information

Chemical Name:C₁₅H₂₀O₄
CAS No.:1268455-58-8
Molecular Formula:C₁₅H₂₀O₄
Molecular Weight:264.321
Hs Code.:

C<sub>15</sub>H<sub>20</sub>O<sub>4</sub>

Synonyms:C₁₅H₂₀O₄

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Chemical Property of C₁₅H₂₀O₄

Chemical Property:

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Technology Process of C₁₅H₂₀O₄

There total 7 articles about C₁₅H₂₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1268455-56-6
C₂₂H₂₄O₄

: 1268455-58-8
C₁₅H₂₀O₄

Guidance literature:: With methanol; camphor-10-sulfonic acid; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/ol1031409

Reference yield:

: 315203-85-1
(2R,4aR,6S,7R,8aS)-2-Phenyl-6-vinyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol

: 1268455-58-8
C₁₅H₂₀O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: ozone / methanol; dichloromethane / -78 °C

1.2: -78 - 0 °C

2.1: 1H-imidazole / tetrahydrofuran; dichloromethane / 1.33 h / 20 °C

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.67 h / 20 °C / Molecular sieve

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C

4.2: 12 h / 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

6.2: 0 - 20 °C

7.1: methanol; camphor-10-sulfonic acid / dichloromethane / 12 h / 20 °C

With 1H-imidazole; methanol; n-butyllithium; tetrapropylammonium perruthennate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hydride; ozone; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil; 4.1: Wittig methylenation / 4.2: Wittig methylenation;
DOI:10.1021/ol1031409

Reference yield:

: 1268455-52-2
C₂₄H₃₈O₄Si

: 1268455-58-8
C₁₅H₂₀O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: methanol; camphor-10-sulfonic acid / dichloromethane / 12 h / 20 °C

With methanol; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol1031409