5-chloro-N-methyl-N-(3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-nitrobenzamide

Base Information

Chemical Name:5-chloro-N-methyl-N-(3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-nitrobenzamide
CAS No.:1394809-98-3
Molecular Formula:C₁₈H₁₅ClN₄O₃
Molecular Weight:370.795
Hs Code.:

Synonyms:5-chloro-N-methyl-N-(3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-nitrobenzamide

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Chemical Property of 5-chloro-N-methyl-N-(3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-nitrobenzamide

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Technology Process of 5-chloro-N-methyl-N-(3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-nitrobenzamide

There total 1 articles about 5-chloro-N-methyl-N-(3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 57047-10-6
3-Methyl-5-methylamino-1-phenyl-1H-pyrazole

: 41994-44-9
5-chloro-2-nitrobenzoyl chloride

: 1394809-98-3
5-chloro-N-methyl-N-(3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-nitrobenzamide

Guidance literature:: 3-Methyl-5-methylamino-1-phenyl-1H-pyrazole; 5-chloro-2-nitrobenzoyl chloride; In chloroform; for 1h; Reflux;

With triethylamine; In chloroform; for 4h; Reflux;
DOI:10.1016/j.ejmech.2012.06.028

Reference yield: 50.0%

: 1394809-98-3
5-chloro-N-methyl-N-(3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-nitrobenzamide

: 1394810-04-8
2-amino-5-chloro-N-methyl-N-(3-methyl-1-phenyl-1H-pyrazol-5-yl)benzamide

Guidance literature:: With iron; acetic acid; In water; at 100 ℃; for 1.75h;
DOI:10.1016/j.ejmech.2012.06.028

Reference yield:

: 1394809-98-3
5-chloro-N-methyl-N-(3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-nitrobenzamide

: (3'SR,4'RS)-5-chloro-4'-hydroxy-2,5'-dimethyl-2'-phenyl-2',4'-dihydrospiro[isoindole-1,3'-pyrazol]-3(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: iron; acetic acid / water / 1.75 h / 100 °C

2.1: sulfuric acid; sodium nitrite / water / 0 - 5 °C

2.2: 1 h / 0 - 20 °C

3.1: water / ethanol / 0.5 h / Reflux

With sulfuric acid; water; iron; acetic acid; sodium nitrite; In ethanol; water; 2.2: Sandmeyer reaction;
DOI:10.1016/j.ejmech.2012.06.028