13H-Dibenzo[a,i]carbazole

Base Information

• Chemical Name: 13H-Dibenzo[a,i]carbazole
• CAS No.: 239-64-5
• Molecular Formula: C20H13 N
• Molecular Weight: 267.33
• Hs Code.: 2933990090
• European Community (EC) Number: 205-949-6
• NSC Number: 109911
• UNII: Q838JL2T8G
• DSSTox Substance ID: DTXSID9075373
• Nikkaji Number: J34.862G
• Wikidata: Q82003323
• Mol file: 239-64-5.mol

Synonyms:13H-Dibenzo[a,i]carbazole;239-64-5;1,2:7,8-Dibenzocarbazole;7H-Dibenzo(a,i)carbazole;1,2,7,8-Dibenzcarbazole;1,2;7,8-Dibenzocarbazole;13H-DIBENZO(A,I)CARBAZOLE;EINECS 205-949-6;dibenzo[a,i]carbazole;Dibenzo(a,i)carbazole;13-Aza-13H-dibenzo(a,i)fluorene;NSC 109911;BRN 0212021;Q838JL2T8G;13-Aza-13H-dibenzo[a,i]fluorene;13(H)-DIBENZO[A,I]CARBAZOLE;NSC-109911;12-azapentacyclo[11.8.0.02,11.05,10.014,19]henicosa-1(13),2(11),3,5,7,9,14,16,18,20-decaene;7H-Dibenzo[a,i]carbazole;NSC109911;Dibenzo[a,j]carbazole;1,8-Dibenzocarbazole;1,7,8-Dibenzcarbazole;UNII-Q838JL2T8G;Oprea1_775391;SCHEMBL5466693;DTXSID9075373;CCG-45347;WLN: T E6 D6 B566 CMJ;LS-60594;SR-01000635123-1;12-azapentacyclo[11.8.0.0?,??.0?,??.0??,??]henicosa-1(21),2,4,6,8,10,13,15,17,19-decaene

Chemical Property of 13H-Dibenzo[a,i]carbazole

Chemical Property:

• Vapor Pressure: 2.39E-11mmHg at 25°C
• Melting Point: 221.3°C
• Refractive Index: 1.8610 (estimate)
• Boiling Point: 544.1°Cat760mmHg
• PKA: 17.00±0.30(Predicted)
• Flash Point: 246.5°C
• PSA: 15.79000
• Density: 1.308g/cm³
• LogP: 5.62750
• Water Solubility.: 10.4ug/L(24 oC)
• XLogP3: 6.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 267.104799419
• Heavy Atom Count: 21
• Complexity: 355

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Chemical Classes: Other Classes -> Polycyclic Aromatic Hydrocarbons
• Canonical SMILES: C1=CC=C2C(=C1)C=CC3=C2NC4=C3C=CC5=CC=CC=C54

Technology Process of 13H-Dibenzo[a,i]carbazole

There total 25 articles about 13H-Dibenzo[a,i]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

6,13-dihydro-5H-dibenzo[a,i]carbazole (63039-79-2) → 13H-dibenzocarbazole (239-64-5)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In acetonitrile; at 20 ℃; for 3h;

Reference yield: 76.0%

1-Nitro-[2,2']binaphthyl (854234-12-1) → 13H-dibenzocarbazole (239-64-5)

Guidance literature:

With triphenylphosphine; In 1,2-dichloro-benzene; at 180 ℃; for 12h;

Reference yield: 75.0%

C20H14ClN → 13H-dibenzocarbazole (239-64-5)

Guidance literature:

With palladium diacetate; potassium carbonate; tri tert-butylphosphoniumtetrafluoroborate; In N,N-dimethyl acetamide; at 90 ℃;

upstream raw materials:

1-Nitronaphthalene

benzo[h]naphtho[1,2-c]cinnoline

6,13-dihydro-5H-dibenzo[a,i]carbazole

[2,2']binaphthyl-1,1'-diyldiamine

Refernces

• 1、 Hodgson,Habeshaw. "-". . p. 1573. Retrieved 1947.
• 2、 -. "COMPOUND FOR ORGANIC ELECTRONIC ELEMENT, ORGANIC ELECTRONIC ELEMENT USING THE SAME, AND AN ELECTRONIC DEVICE THEREOF". Paragraph 0525; 0562-0564; 0567-0568; 0582-0583; 0587-0588. . Retrieved 2020/05/26.
• 3、 -. "ORGANIC COMPOUNDS AND ORGANIC ELECTRO LUMINESCENCE DEVICE COMPRISING THE SAME". Paragraph 0119; 0127-0131. . Retrieved 2019/07/29.