(S)-3-(benzyloxy)propane-1,2-diyl bis(10-((2E,4E)-hexa-2,4-dienoyloxy)decanoate)

Base Information

Chemical Name:(S)-3-(benzyloxy)propane-1,2-diyl bis(10-((2E,4E)-hexa-2,4-dienoyloxy)decanoate)
CAS No.:1314897-91-0
Molecular Formula:C₄₂H₆₂O₉
Molecular Weight:710.949
Hs Code.:

Synonyms:(S)-3-(benzyloxy)propane-1,2-diyl bis(10-((2E,4E)-hexa-2,4-dienoyloxy)decanoate)

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Chemical Property of (S)-3-(benzyloxy)propane-1,2-diyl bis(10-((2E,4E)-hexa-2,4-dienoyloxy)decanoate)

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Technology Process of (S)-3-(benzyloxy)propane-1,2-diyl bis(10-((2E,4E)-hexa-2,4-dienoyloxy)decanoate)

There total 4 articles about (S)-3-(benzyloxy)propane-1,2-diyl bis(10-((2E,4E)-hexa-2,4-dienoyloxy)decanoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 56552-80-8
(R)-3-benzyloxy-1,2-propanediol

: 137794-52-6
10-((2E,4E)-hexa-2,4-dienoyloxy)decanoic acid

: 1314897-91-0
(S)-3-(benzyloxy)propane-1,2-diyl bis(10-((2E,4E)-hexa-2,4-dienoyloxy)decanoate)

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetlet.2010.11.090

Reference yield:

: 110-44-1,91751-55-2
sorbic Acid

: 1314897-91-0
(S)-3-(benzyloxy)propane-1,2-diyl bis(10-((2E,4E)-hexa-2,4-dienoyloxy)decanoate)

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / dichloromethane / 20 °C / Cooling with ice

1.2: 20 °C

2.1: pyridine; potassium cyanide; lithium iodide / 24 h / 120 °C

3.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C

With pyridine; dmap; potassium cyanide; 2,4,6-trichlorobenzoyl chloride; triethylamine; dicyclohexyl-carbodiimide; lithium iodide; In dichloromethane; 1.1: Yamaguchi reaction / 1.2: Yamaguchi reaction;
DOI:10.1016/j.tetlet.2010.11.090

Reference yield:

: 1314897-83-0
methyl 10-((2E,4E)-hexa-2,4-dienoyloxy)decanoate

: 1314897-91-0
(S)-3-(benzyloxy)propane-1,2-diyl bis(10-((2E,4E)-hexa-2,4-dienoyloxy)decanoate)

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; potassium cyanide; lithium iodide / 24 h / 120 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C

With pyridine; dmap; potassium cyanide; dicyclohexyl-carbodiimide; lithium iodide; In dichloromethane;
DOI:10.1016/j.tetlet.2010.11.090