biphenyl-4-yl 2,4,6-tri-O-benzoyl-3-O-(dibenzyloxyphosphoryl)-α-D-mannopyranoside

Base Information

Chemical Name:biphenyl-4-yl 2,4,6-tri-O-benzoyl-3-O-(dibenzyloxyphosphoryl)-α-D-mannopyranoside
CAS No.:1415481-53-6
Molecular Formula:C₅₃H₄₅O₁₂P
Molecular Weight:904.907
Hs Code.:

Synonyms:biphenyl-4-yl 2,4,6-tri-O-benzoyl-3-O-(dibenzyloxyphosphoryl)-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of biphenyl-4-yl 2,4,6-tri-O-benzoyl-3-O-(dibenzyloxyphosphoryl)-α-D-mannopyranoside

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Technology Process of biphenyl-4-yl 2,4,6-tri-O-benzoyl-3-O-(dibenzyloxyphosphoryl)-α-D-mannopyranoside

There total 2 articles about biphenyl-4-yl 2,4,6-tri-O-benzoyl-3-O-(dibenzyloxyphosphoryl)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1415481-52-5
biphenyl-4-yl 2,4,6-tri-O-benzoyl-α-D-mannopyranoside

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 1623-08-1
phosphoric acid dibenzyl ester

: 1415481-53-6
biphenyl-4-yl 2,4,6-tri-O-benzoyl-3-O-(dibenzyloxyphosphoryl)-α-D-mannopyranoside

Guidance literature:: biphenyl-4-yl 2,4,6-tri-O-benzoyl-α-D-mannopyranoside; Dibenzyl N,N-diisopropylphosphoramidite; With 1,2,4-Triazole; In acetonitrile; at 0 - 20 ℃; for 24.3333h;

With tert.-butylhydroperoxide; In acetonitrile; at 0 - 20 ℃; for 1h;

Reference yield:

: 1415481-52-5
biphenyl-4-yl 2,4,6-tri-O-benzoyl-α-D-mannopyranoside

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 1415481-53-6
biphenyl-4-yl 2,4,6-tri-O-benzoyl-3-O-(dibenzyloxyphosphoryl)-α-D-mannopyranoside

: C₅₃H₄₅O₁₂P

Guidance literature:: biphenyl-4-yl 2,4,6-tri-O-benzoyl-α-D-mannopyranoside; Dibenzyl N,N-diisopropylphosphoramidite; With 1,2,4-Triazole; In acetonitrile; at 0 - 20 ℃;

With tert.-butylhydroperoxide; In water; acetonitrile; at 20 ℃; for 1h; Overall yield = 80 %; Overall yield = 245 mg;
DOI:10.1021/acs.jmedchem.5b01923

Reference yield:

: 1415481-53-6
biphenyl-4-yl 2,4,6-tri-O-benzoyl-3-O-(dibenzyloxyphosphoryl)-α-D-mannopyranoside

: 1415481-54-7
C₃₉H₃₃O₁₂P

Guidance literature:: With phosphoric acid dibenzyl ester; hydrogen; 10% palladium hydroxide on charcoal; In ethyl acetate; at 20 ℃; for 5h; under 760.051 Torr;