(Z)-2-(bromomethyl)-N-(tert-butylcarbamoyl)-N-phenethyl-3-o-tolylacrylamide

Base Information

Chemical Name:(Z)-2-(bromomethyl)-N-(tert-butylcarbamoyl)-N-phenethyl-3-o-tolylacrylamide
CAS No.:1394001-79-6
Molecular Formula:C₂₄H₂₉BrN₂O₂
Molecular Weight:457.41
Hs Code.:

Synonyms:(Z)-2-(bromomethyl)-N-(tert-butylcarbamoyl)-N-phenethyl-3-o-tolylacrylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(bromomethyl)-N-(tert-butylcarbamoyl)-N-phenethyl-3-o-tolylacrylamide

Chemical Property:

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Technology Process of (Z)-2-(bromomethyl)-N-(tert-butylcarbamoyl)-N-phenethyl-3-o-tolylacrylamide

There total 3 articles about (Z)-2-(bromomethyl)-N-(tert-butylcarbamoyl)-N-phenethyl-3-o-tolylacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₁₁BrO₂

: 1258239-64-3
2-methyl-N-((phenethylimino)methylene)propan-2-amine

: 1394001-80-9
(Z)-2-(bromomethyl)-N-tert-butyl-N-(phenethylcarbamoyl)-3-o-tolylacrylamide

: 1394001-79-6
(Z)-2-(bromomethyl)-N-(tert-butylcarbamoyl)-N-phenethyl-3-o-tolylacrylamide

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetlet.2012.06.109

Reference yield:

: 1019376-91-0
ethyl 2-((hydroxy)(o-tolyl)methyl)acrylate

: 1394001-80-9
(Z)-2-(bromomethyl)-N-tert-butyl-N-(phenethylcarbamoyl)-3-o-tolylacrylamide

: 1394001-79-6
(Z)-2-(bromomethyl)-N-(tert-butylcarbamoyl)-N-phenethyl-3-o-tolylacrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / methanol; water

2: dichloromethane / 20 °C

With potassium hydroxide; In methanol; dichloromethane; water;
DOI:10.1016/j.tetlet.2012.06.109

Reference yield:

: 529-20-4
2-methylphenyl aldehyde

: 1394001-80-9
(Z)-2-(bromomethyl)-N-tert-butyl-N-(phenethylcarbamoyl)-3-o-tolylacrylamide

: 1394001-79-6
(Z)-2-(bromomethyl)-N-(tert-butylcarbamoyl)-N-phenethyl-3-o-tolylacrylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1,4-diaza-bicyclo[2.2.2]octane

2: potassium hydroxide / methanol; water

3: dichloromethane / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; potassium hydroxide; In methanol; dichloromethane; water; 1: Baylis-Hillman reaction;
DOI:10.1016/j.tetlet.2012.06.109