lobarin

Base Information

Chemical Name:lobarin
CAS No.:1372167-27-5
Molecular Formula:C₂₅H₃₀O₉
Molecular Weight:474.508
Hs Code.:

Synonyms:lobarin

Suppliers and Price of lobarin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of lobarin

Chemical Property:

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Technology Process of lobarin

There total 19 articles about lobarin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: benzyl 4,6-bis(benzyloxy)-3-((1-butyl-1-hydroxy-6-methoxy-3-oxo-1,3-dihydroisobenzofuran-4-yl)oxy)-2-pentylbenzoate

: 1372167-27-5
lobarin

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 12h;

Reference yield: 93.0%

: 522-53-2
lobaric acid

: 1372167-27-5
lobarin

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 3-butyl-3-hydroxy-7-iodo-5-methoxyisobenzofuran-1-(3H)-one

: 1372167-27-5
lobarin

Guidance literature:: Multi-step reaction with 2 steps

1: potassium phosphate; copper(l) iodide / dimethyl sulfoxide / 12 h / 110 °C / Inert atmosphere

2: hydrogen; palladium 10% on activated carbon / methanol / 12 h / 760.05 Torr

With potassium phosphate; copper(l) iodide; palladium 10% on activated carbon; hydrogen; In methanol; dimethyl sulfoxide; 1: |Ullmann Condensation;
DOI:10.1021/acs.jnatprod.8b00227