tert-butyl 2-(3-(3-chlorophenyl)prop-2-ynyl)-3-methyl-2H-azirine-2-carboxylate

Base Information

Chemical Name:tert-butyl 2-(3-(3-chlorophenyl)prop-2-ynyl)-3-methyl-2H-azirine-2-carboxylate
CAS No.:1627205-33-7
Molecular Formula:C₁₇H₁₈ClNO₂
Molecular Weight:303.788
Hs Code.:

Synonyms:tert-butyl 2-(3-(3-chlorophenyl)prop-2-ynyl)-3-methyl-2H-azirine-2-carboxylate

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Chemical Property of tert-butyl 2-(3-(3-chlorophenyl)prop-2-ynyl)-3-methyl-2H-azirine-2-carboxylate

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Technology Process of tert-butyl 2-(3-(3-chlorophenyl)prop-2-ynyl)-3-methyl-2H-azirine-2-carboxylate

There total 5 articles about tert-butyl 2-(3-(3-chlorophenyl)prop-2-ynyl)-3-methyl-2H-azirine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: C₂₄H₂₆ClNO₅S

: 1627205-33-7
tert-butyl 2-(3-(3-chlorophenyl)prop-2-ynyl)-3-methyl-2H-azirine-2-carboxylate

Guidance literature:: With triethylamine;
DOI:10.1002/anie.201402470

Reference yield:

: 1627205-20-2
C₁₇H₁₉ClO₃

: 1627205-33-7
tert-butyl 2-(3-(3-chlorophenyl)prop-2-ynyl)-3-methyl-2H-azirine-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; hydroxylamine hydrochloride / 50 °C

2: pyridine / dichloromethane / 20 °C / Inert atmosphere

3: triethylamine

With pyridine; hydroxylamine hydrochloride; triethylamine; In dichloromethane;
DOI:10.1002/anie.201402470

Reference yield:

: 80250-03-9
tert-butyl 2-acetylpent-4-ynoate

: 1627205-33-7
tert-butyl 2-(3-(3-chlorophenyl)prop-2-ynyl)-3-methyl-2H-azirine-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 50 °C / Inert atmosphere

2: pyridine; hydroxylamine hydrochloride / 50 °C

3: pyridine / dichloromethane / 20 °C / Inert atmosphere

4: triethylamine

With pyridine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydroxylamine hydrochloride; triethylamine; In dichloromethane;
DOI:10.1002/anie.201402470