9-(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)-9-germaanthracene

Base Information

Chemical Name:9-(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)-9-germaanthracene
CAS No.:904911-47-3
Molecular Formula:C₄₃H₇₆GeSi₇
Molecular Weight:862.265
Hs Code.:

Synonyms:9-(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)-9-germaanthracene

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Chemical Property of 9-(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)-9-germaanthracene

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Technology Process of 9-(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)-9-germaanthracene

There total 6 articles about 9-(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)-9-germaanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 904911-55-3
9-trifluoromethanesulfonyl-9-(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)-9,10-dihydro-9-germaanthracene

: 904911-47-3
9-(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)-9-germaanthracene

Guidance literature:: With lithium diisopropylamide; In benzene; room temp.;
DOI:10.1021/om060371+

Reference yield:

: 61592-89-0
2,2’-dibromodiphenylmethane

: 904911-47-3
9-(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)-9-germaanthracene

Guidance literature:: Multi-step reaction with 5 steps

1: n-butyllithium / diethyl ether

2: tetrahydrofuran

3: BPO / benzene

4: dichloromethane

5: lithium diisopropylamide / benzene

With n-butyllithium; BPO; lithium diisopropylamide; In tetrahydrofuran; diethyl ether; dichloromethane; benzene;
DOI:10.1021/om060371+

Reference yield:

: 904911-60-0
((CH₃)3Si)3C(((CH₃)3Si)2CH)2C₆H₂GeCl₃

: 904911-47-3
9-(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)-9-germaanthracene

Guidance literature:: Multi-step reaction with 5 steps

1: n-butyllithium / diethyl ether

2: tetrahydrofuran

3: BPO / benzene

4: dichloromethane

5: lithium diisopropylamide / benzene

With n-butyllithium; BPO; lithium diisopropylamide; In tetrahydrofuran; diethyl ether; dichloromethane; benzene;
DOI:10.1021/om060371+