((4-fluorophenyl)(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)trimethylsilane

Base Information

Chemical Name:((4-fluorophenyl)(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)trimethylsilane
CAS No.:1535207-53-4
Molecular Formula:C₁₆H₂₆BFO₂Si
Molecular Weight:308.276
Hs Code.:

Synonyms:((4-fluorophenyl)(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)trimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((4-fluorophenyl)(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)trimethylsilane

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Technology Process of ((4-fluorophenyl)(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)trimethylsilane

There total 4 articles about ((4-fluorophenyl)(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)trimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1765-93-1
4-fluoroboronic acid

: 18107-18-1
diazomethyl-trimethyl-silane

: 1535207-53-4
((4-fluorophenyl)(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)trimethylsilane

Guidance literature:: 4-fluoroboronic acid; diazomethyl-trimethyl-silane; In toluene; at 100 ℃; for 4h; Inert atmosphere; Schlenk technique;

2,3-dimethyl-2,3-butane diol; With water; In toluene; at 100 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c9ob01006h

Reference yield: 71.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 448-59-9
tris(4-fluorophenyl)boroxine

: 18107-18-1
diazomethyl-trimethyl-silane

: 1535207-53-4
((4-fluorophenyl)(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)trimethylsilane

Guidance literature:: tris(4-fluorophenyl)boroxine; diazomethyl-trimethyl-silane; With N-ethyl-N,N-diisopropylamine; In hexane; toluene; at 85 ℃; for 1h; Inert atmosphere;

2,3-dimethyl-2,3-butane diol; In hexane; toluene; at 20 ℃; Inert atmosphere;
DOI:10.1039/c7sc02264f

Reference yield: 65.0%

: 1535207-45-4
(bis(4,4,5,5‐tetramethyl‐1,3,2‐dioxaborolan‐2‐yl)methyl)trimethylsilane

: 460-00-4
1-Bromo-4-fluorobenzene

: 1535207-53-4
((4-fluorophenyl)(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)trimethylsilane

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; potassium hydroxide; silver(l) oxide; In 1,4-dioxane; water; at 20 ℃; for 3.5h; chemoselective reaction;
DOI:10.1246/cl.130643