Technology Process of 2-(phenylsulfonyl)-5,5-dimethyl-1-hexene
There total 5 articles about 2-(phenylsulfonyl)-5,5-dimethyl-1-hexene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
for 0.166667h;
Ambient temperature;
DOI:10.1021/jo00247a006
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) n-butyllithium, 2.) hexamethylphosphoric triamide (HMPA) / 1.) hexane, diethyl ether, -70 deg C, 25 min, 2.) hexane, diethyl, RT, 2 h
2: 1.) n-butyllithium, 2.) tert-butyl hypochlorite / 1.) diethyl ether, hexane, -70 deg C, 45 min, 2.) diethyl ether, hexane
3: 100 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.17 h / Ambient temperature
With
N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; tert-butylhypochlorite; tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
DOI:10.1021/jo00247a006
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) n-butyllithium, 2.) hexamethylphosphoric triamide (HMPA) / 1.) hexane, diethyl ether, -70 deg C, 25 min, 2.) hexane, diethyl, RT, 2 h
2: 1.) n-butyllithium, 2.) tert-butyl hypochlorite / 1.) diethyl ether, hexane, -70 deg C, 45 min, 2.) diethyl ether, hexane
3: 100 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.17 h / Ambient temperature
With
N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; tert-butylhypochlorite; tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
DOI:10.1021/jo00247a006
