2-Diethylamino-N-[2,6-dimethyl-4-(toluene-4-sulfonylamino)-phenyl]-butyramide

Base Information

Chemical Name:2-Diethylamino-N-[2,6-dimethyl-4-(toluene-4-sulfonylamino)-phenyl]-butyramide
CAS No.:83473-45-4
Molecular Formula:C₂₃H₃₃N₃O₃S
Molecular Weight:431.599
Hs Code.:

Synonyms:2-Diethylamino-N-[2,6-dimethyl-4-(toluene-4-sulfonylamino)-phenyl]-butyramide

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Chemical Property of 2-Diethylamino-N-[2,6-dimethyl-4-(toluene-4-sulfonylamino)-phenyl]-butyramide

Chemical Property:

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Technology Process of 2-Diethylamino-N-[2,6-dimethyl-4-(toluene-4-sulfonylamino)-phenyl]-butyramide

There total 4 articles about 2-Diethylamino-N-[2,6-dimethyl-4-(toluene-4-sulfonylamino)-phenyl]-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 98-59-9
p-toluenesulfonyl chloride

: 83473-72-7
N-(4-Amino-2,6-dimethyl-phenyl)-2-diethylamino-butyramide

: 83473-45-4
2-Diethylamino-N-[2,6-dimethyl-4-(toluene-4-sulfonylamino)-phenyl]-butyramide

Guidance literature:: With pyridine; In dichloromethane; at 0 - 5 ℃;
DOI:10.1002/jps.2600710619

Reference yield:

: 16947-63-0
2,6-dimethyl-4-nitroaniline

: 83473-45-4
2-Diethylamino-N-[2,6-dimethyl-4-(toluene-4-sulfonylamino)-phenyl]-butyramide

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / PCl₃ / benzene / 3 h / Heating

2: 47 percent / NaHCO₃ / benzene / Heating

3: 82 percent / Fe, conc. HCl / ethanol; H₂O / 0.58 h / Heating

4: 81 percent / pyridine / CH₂Cl₂ / 0 - 5 °C

With pyridine; hydrogenchloride; iron; sodium hydrogencarbonate; phosphorus trichloride; In ethanol; dichloromethane; water; benzene;
DOI:10.1002/jps.2600710619

Reference yield:

: 2-Chloro-N-(2,6-dimethyl-4-nitro-phenyl)-butyramide

: 83473-45-4
2-Diethylamino-N-[2,6-dimethyl-4-(toluene-4-sulfonylamino)-phenyl]-butyramide

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / NaHCO₃ / benzene / Heating

2: 82 percent / Fe, conc. HCl / ethanol; H₂O / 0.58 h / Heating

3: 81 percent / pyridine / CH₂Cl₂ / 0 - 5 °C

With pyridine; hydrogenchloride; iron; sodium hydrogencarbonate; In ethanol; dichloromethane; water; benzene;
DOI:10.1002/jps.2600710619