[(2R,3R,4S,5R,6S)-4,5-Bis-benzyloxy-3-((2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy)-6-methoxy-tetrahydro-pyran-2-yl]-methanol

Base Information

• Chemical Name: [(2R,3R,4S,5R,6S)-4,5-Bis-benzyloxy-3-((2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy)-6-methoxy-tetrahydro-pyran-2-yl]-methanol
• CAS No.: 83565-29-1
• Molecular Formula: C₅₄H₅₈O₁₀Se
• Molecular Weight: 946.009

Synonyms:[(2R,3R,4S,5R,6S)-4,5-Bis-benzyloxy-3-((2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy)-6-methoxy-tetrahydro-pyran-2-yl]-methanol

Chemical Property of [(2R,3R,4S,5R,6S)-4,5-Bis-benzyloxy-3-((2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy)-6-methoxy-tetrahydro-pyran-2-yl]-methanol

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Technology Process of [(2R,3R,4S,5R,6S)-4,5-Bis-benzyloxy-3-((2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy)-6-methoxy-tetrahydro-pyran-2-yl]-methanol

There total 1 articles about [(2R,3R,4S,5R,6S)-4,5-Bis-benzyloxy-3-((2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy)-6-methoxy-tetrahydro-pyran-2-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Benzoic acid (2R,3R,4S,5R,6S)-4,5-bis-benzyloxy-3-((2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy)-6-methoxy-tetrahydro-pyran-2-ylmethyl ester → [(2R,3R,4S,5R,6S)-4,5-Bis-benzyloxy-3-((2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy)-6-methoxy-tetrahydro-pyran-2-yl]-methanol (83565-29-1)

Guidance literature:

With sodium methylate; In methanol;

DOI:10.1039/c39820000701

Reference yield:

[(2R,3R,4S,5R,6S)-4,5-Bis-benzyloxy-3-((2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy)-6-methoxy-tetrahydro-pyran-2-yl]-methanol (83565-29-1) → C54H58O11Se

Guidance literature:

With sodium periodate; In methanol; water; at 20 ℃; for 1h; Yield given;

DOI:10.1039/c39820000701

Reference yield:

[(2R,3R,4S,5R,6S)-4,5-Bis-benzyloxy-3-((2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy)-6-methoxy-tetrahydro-pyran-2-yl]-methanol (83565-29-1) → C48H52O10

Guidance literature:

Multi-step reaction with 2 steps

1: sodium periodate / methanol; H₂O / 1 h / 20 °C

2: 61.5 percent / di-isopropylamine / various solvent(s) / 2 h / Heating

With sodium periodate; diisopropylamine; In methanol; water;

DOI:10.1039/c39820000701

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